O-97 Oxidation of camphor ethylene dithioacetal [Electronic resource] / A. V. Timshina, S. A. Rubtsova, I. N. Alekseev, P. A. Slepukhin, A. V. Kuchin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2010. - Vol. 46, № 3. - P363-367 . - Springerlink.com Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: (1R,1R,2S,4R)-1,7,7-Trimethylspiro[bicyclo[2.2.1]heptane-2,2?-[1,3]dithiolane] 1-oxide, (1R,2S,3R,4R)-1,7,7-trimethylspiro[bicyclo[2.2.1]heptane-2,2-[1,3]dithiolane] 1,1,3-trioxide, and (1R,4R)-1,7,7-trimethylspiro[bicyclo[2.2.1]heptane-2,2?-[1,3]dithiolane] 1,1,3,3-tetraoxide were synthesized by oxidation of camphor ethylene dithioacetal with m-chloroperoxybenzoic acid at different substrate-tooxidant ratios. The structure of the products was proved by IR and NMR spectroscopy and X-ray analysis \\\\Expert2\\nbo\\Russian Journal of Organic Chemistry\\2010, 46 (3), 363.pdf |