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Труды Института высокотемпературной электрохимии УрО РАН
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Труды сотрудников Института горного дела УрО РАН
Труды сотрудников Института органического синтеза УрО РАН
Труды сотрудников Института теплофизики УрО РАН
Труды сотрудников Института химии твердого тела УрО РАН
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Труды сотрудников ЦНБ УрО РАН
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Общее количество найденных документов : 100
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1.
Инвентарный номер: нет.
   
   N 64

    Nikitin, E. D.
    Vapor-Liquid Critical Properties of Phenol and (C8 to C10) Phenylalkanols [Text] / E. D. Nikitin, A. M. Popov, Yu. G. Yatluk // Journal of Chemical & Engineering Data. - 2007. - Vol. 52, № 1. - P315-317
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: The critical pressures and temperatures of phenol and three phenylalkanols C6H5(CH2)nOH with n = 2 to 4 have been measured. These substances are thermally unstable at their critical points. The pulse-heating method with ultralow residence times has been used. Residence times are from (0.03 to 1) ms. The experimental critical properties of phenol and phenylalkanols have been compared with the values calculated using the group-contribution methods by Constantinou and Gani and by Marrero and Gani

\\\\Expert2\\nbo\\Journal of Chemical and Engineering Data\\2007, v.52, p.315.pdf
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2.
Инвентарный номер: нет.
   
   U 92

   
    Utilization of polychlorinated biphenyls with the use of chemical and biological processes [Electronic resource] / D. O. Egorova, E. G. Plotnikiva, A. V. Mekhaev, Yu. G. Yatluk, V. A. Demakov, O. N. Chupakhin // Doklady Chemistry. - 2011. - Vol.441, №1. - P334-337
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
POLYCHLORINATED BIPHENYLS -- UTILIZATION

\\\\Expert2\\nbo\\Doklady Chemistry\\2011, v. 441, N 1, p. 334-337.pdf
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3.
Инвентарный номер: нет.
   
   U 88

   
    Use of low-molecular polyacrylic acid as the dispersant of Nd3+, Yb3+ doped Y2O3 nanoparticles for slip casting and sintering of laser ceramics [Text] / I. Puzyrev, M. Ivanov, V. Osipov, Yu. G. Yatluk // Nanotech Insight 2007 : The International conference on Nanotechnology, Luxor, Egypt, 10-17 march 2007 : abstr. . - Luxor, Egypt, 2007. - P310-311 : табл. - Bibliogr. : p. 311 (3 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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4.
Инвентарный номер: нет.
   
   U 52

   
    Unexpexted isomerization in the series of fluorine-containing 2,3-dihydro-1H-1,4-diazepines with a 2-aminoethyl group at one of the nitrogen atoms [Electronic resource] / V. Ya. Sosnovskikh, I. I. Vorontsov, V. A. Kutsenko, Yu. G. Yatluk // Mendeleev Communications. - 2000. - Vol. 10, N 2. - P56-58 . - ISSN 0959-9436
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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5.
Инвентарный номер: нет.
   
   P 49

    Pestov, A. V.
    Triocarbaamoylation of chitosan [] : доклад, тезисы доклада / A. V. Pestov, Yu. A. Skorik, Yu. G. Yatluk // 10-th International Conference on Chitin and Chitosan - 7th International Conference of the European Chitin Society, Le Corum, Montpellier, France, 6-9 September 2006 : book of abstracts . - Le Corum, Montpellier (France), 2006. - 76 (PC 12)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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6.
Инвентарный номер: нет.
   
   T 45

   
    Thiocarbamoyl chitosan as a novel sorbent with high sorption capacity and selectivity for the ions of gold(III), platinum(IV), and palladium [Electronic resource] / A. V. Pestov, S. Yu. Bratskaya, A. Slobodyuk, V. A. Avramenko, Yu. G. Yatluk // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2010. - Vol. 59, № 7. - P1303-1306
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CHITOSAN -- THIOCARBAMOYL CHITOSAN -- IONS OF GOLD(III)
Аннотация: Thiocarbamoyl chitosan (TCC) was synthesized by grafting thiourea on chitosan backbone in eutectic composition of ammonium thiocyanate—thiourea. Insoluble products with the amno group functionalization degree of 0.3–1.1 can be prepared by varying the conditions of polymer-analogous (synthesis in a gel) transformation. Structure of the synthesized chitosan derivatives was characterized by elemental analysis, diffuse reflectance infrared spectroscopy, and the solid state 13C NMR. Study of sorption properties of TCC shows high sorption capacity and selectivity for the ions of gold(III), platinum(IV), and palladium(II) as evidenced by results obtained at pH 2 in the presence of 100–1000-fold excess of iron(III), copper(II), zinc(II), and nickel(II). Sorption capacity of TCC for all ions increases with the increase in the degree of substitution and changes in the series: AuIII > PdII > PtIV

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2010, 59 (7), 1303-1306.pdf
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7.
Инвентарный номер: нет.
   
   T 44

   
    Thermal stability of new sorption materials based on polysiloxanes / L. K. Neudachina, A. Y. Golub, E. M. Gorbunova, Yu. G. Yatluk // Glass Physics and Chemistry. - 2011. - Vol.37, №6. - С. 603-612
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
THERMAL STABILITY -- THIOCARBAMOYLATED POLYSILOXANES -- SILOXANE MATRIX
Аннотация: The thermal stability of the unmodified, aminated, and thiocarbamoylated polysiloxanes has been studied. The siloxane matrix is stable in the temperature range up to 800°C. For the first time, mass spectrometry has been applied to the analysis of the composition of the gaseous products of thermal decomposition of the studied polysiloxanes. It has been shown that, in the process of thermal decomposition, the terminal functional groups are detached and oxidized. Water, ammonia, nitrogen, carbon, and sulfur (in the case of thiourea-modified sorbent) oxides are formed predominantly. The quantitative removal of functional groups during heating up to 800°C has been confirmed by IR spectroscopy. A mechanism of thermal decomposition of polysiloxane xerogels has been proposed. It has been found that adsorption of platinum increases the thermal stability of the samples

\\\\Expert2\\nbo\\Glass Physics and Chemistry\\2011, V. 37, N 6, P.603-612.pdf
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8.
Инвентарный номер: нет.
   
   T 44

   
    The first cubane-like complex of copper based on N -carboxyethyl-tris(hydroxymethyl)aminomethane: Synthesis and crystal structure [Electronic resource] / A. V. Pestov, A. V. Virovets, N. V. Podberezskaya, Yu. G. Yatluk // Russian Journal of Coordination Chemistry. - 2008. - Vol. 34, № 1. - P1-7. - Bibliogr. : p. 7 (9 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: The interaction of acrylic acid with tris(hydroxymethyl)aminomethane (I) was studied. A simple method was suggested for preparing N-carboxyethyl-tris(hydroxymethyl)aminomethane (homotricin) (II). On the basis of compound II, the 1:1 Cu complex, [Cu(OCH2C(CH2OH)2NHCH2CH2COO)]4·nH2O (n = 4–11.25) (III), which is alkoxycarboxylate, was synthesized. The crystal structure of III was found to correspond to a cubane-like tetranuclear cluster (an automated Bruker X8Apex diffractometer with CCD detector (MoK radiation, graphite monochromator, v = 1.11°-27.5°), 8016 reflections, space group P , a = 12.5573(3), b = 19.1012(4), c = 21.2903(5) A, a = 80.7770(10)°, beta = 75.7430(10)°, y = 75.2260(10)°, V = 4761.62(19) A3, p(calcd.) = 1.704 g/cm3, Z = 4). The crystals are unstable due to the large number of water molecules

\\\\Expert2\\nbo\\Russian Journal of Coordination Chemistry\\2008, v. 34, N. 1, p.1.pdf
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9.
Инвентарный номер: нет.
   
   T 44

   
    The effect of acrylic copolymer on viscosity and stability of suspensions of the nanopowders YSZ in isopropanol [Text] / I. Puzyrev, A. S. Lipilin, V. Ivanov, Yu. G. Yatluk // Nanotech Insight 2007 : The International conference on Nanotechnology, Luxor, Egypt, 10-17 march 2007 : abstr. . - Luxor, Egypt, 2007. - P311-313. - Bibliogr. : p. 313 (2 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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10.
Инвентарный номер: нет.
   
   T 44

   
    The catalytic activity of functional polisiloxans in reaction of liquid-phase oxidizing dehydrogenation of hydroxyarens [Text] / Yu. A. Berdugin, Yu. V. Mikushina, V. G. Kharchuk, L. A. Petrov, Yu. G. Yatluk // III International Conference "Catalysis : Fundamentals and Application", dedeicated to the 100-th anniversary of Academician Georgii K. Boreskov : abstr. - Novosibirsk, Russia, 2007. - Vol. I. - P187-188. - Bibliogr. : p. 188 (2 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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11.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis, characterization and some properties of N-(2-carboxyethyl)chitosan [Text] / Yu. A. Skorik, C. A. R. Gomes, M. T.S.D. Vasconcelos, Yu. G. Yatluk // Advances in Chitin Science : Proceedings of the 5th Asia Pacific Chitin and Chitosan Symposium & Exhibition, Bangkok, Thailand, March 13-15, 2002. - Bangkoki, 2002. - Vol. 5. - P344+348 : il. - Bibliogr. : p. 348 (19 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CHITOSAN -- CARBOXYETHYL -- ALKYLATION -- POLYAMPHOLYTE -- POTENTIOMETRIC TITRATION -- PROTONATION CONSTANTS

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12.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis, characterization and application of a new modified polysiloxane with grafted 2-aminoethylpyridine functional groups [Text] / A. S. Zasuhin, L. K. Neudachina, Yu. S. Moskaleva, O. A. Osipova, Yu. G. Yatluk // Modern problems of Surface Chemistry and Physics : International Symposium devoted to the 80th anneversary of Academician O. O. Chuiko, Kyiv, 18-21 May 2010 : abstracts. - Kyiv, 2010. - P350-351 : il.
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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13.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis of poly[N-(2,3-dihydroxypropyl)aminostyrene], a new sorbent for boron(III) ions / D. V. Nesterov, L. S. Molochnikov, M. I. Kodess, E. G. Matochkina, O. V. Koryakova, Yu. G. Yatluk, A. V. Pestov // Russian Journal of Applied Chemistry. - 2013. - Vol.86, №5. - С. 777-781. - Библиогр.: с. 781 (33 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
AMINOSTYRENE -- NITRATION -- GLYCIDOL
Аннотация: A procedure was developed for preparation of poly[N-(2,3-dihydroxypropyl)aminostyrene] via successive stages of nitration, reduction, and glycidol treatment of polystyrene, which gives the polymer with a maximal degree of functionalization. The composition and structure of the intermediates and end products of the polymer-analogous reactions were characterized by elemental analysis, IR spectroscopy, and solid-state 13C NMR spectroscopy. The sorption characteristics of poly[N-(2,3-dihydroxypropyl)aminostyrene] toward boroncontaining ions were assessed

\\\\expert2\\NBO\\Russian Journal of Applied Chemistry\\2013, v. 86, N 5, p.777.pdf
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14.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis of Esters in the Presence of Chlorosilanes [Electronic resource] / V. V. Kozhukova, S. A. Kalyuzhnaya, Yu. G. Yatluk, A. L. Suvorov // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2004. - Vol. 40, № 6. - P773-774
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Esterification of various carboxylic acids with primary alcohols in the presence of chloro(methyl)-silanes provides a simple and convenient synthetic route to esters??

\\\\Expert2\\nbo\\Russian Journal of Organic Chemistry\\2004, 40 (6), 773.pdf
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15.
Инвентарный номер: нет.
   
   K 96

    Kuznetsov, V. A.
    Synthesis of epsilon-caprolactone with stable hydrogen peroxide adducts / V. A. Kuznetsov, M. G. Pervova, Yu. G. Yatluk // Russian Journal of Applied Chemistry. - 2013. - Vol.86, №2. - С. 176-181. - Библиогр.: с. 181 (16 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CYCLOHEXANONE -- E-CAPROLACTONE -- HEXAFLUOROISOPROPANOL
Аннотация: Oxidation of cyclohexanone to ɛ-caprolactone with stable industrially manufactured hydrogen peroxide derivatives: adduct with urea (urea hydrogen peroxide), sodium perborate, sodium percarbonate (Persol), magnesium monoperphthalate (Dismozon) was studied. Oxidation with urea hydrogen peroxide is the most efficient in hexafluoroisopropanol in the case of preliminary removal of urea in the form of an oxalate. Oxidation with sodium perborate and percarbonate provides high yields in trifluoroacetic acid. The lowest cost process consists in interaction with sodium monoperphthalate (Persol and phthalic anhydride) in an aqueous medium

\\\\expert2\\NBO\\Russian Journal of Applied Chemistry\\2013, v. 86, N 2, p.176.pdf
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16.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis of chelating polymer sorbents by using the S-N(H) methodology / A. V. Pestov, P. A. Slepukhin, Yu. G. Yatluk, V. N. Charushin, O. N. Chupakhin // Journal of Applied Polymer Science . - 2012. - Vol.125, №3. - С. 1970-1978
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
FUNCTIONALIZATION OF POLYMERS -- PHENOL -- X-RAY ANALYSIS
Аннотация: The article describes a new synthetic approach to modify the structure of phenol-formaldehyde and resorcinol-formaldehyde resins, which enables one to functionalize a polymer matrix by using the S?NH (nucleophilic aromatic substitution of hydrogen) methodology. Direct heteroarylation of phenol (resorcinol) fragments in polymer chains with 1,2,4-triazine derivatives illustrates a new synthetic method in the polymer chemistry. The feature of this methodology is that it provides an opportunity to accomplish direct one-pot polymer transformations by incorporating of rather complicated chelating groups through the displacement of hydrogen in phenol moieties. It has been shown that in order to obtain chemically modified polymers on the basis of phenol-formaldehyde and resorcinol-formaldehyde resins with a high degree of substitution with chelating units, a polymer matrix has to react with 3-(pyridin-2'-yl)-1,2,4-triazin-5(2H)-one. Also, it has been found that polymer sorbents with a high selectivity can be obtained by using the template method. Targeted synthesis of model compounds, as structural units of the chelating polymers, and elucidation of the structure of their complexes with copper (II) ions have shown that the most plausible type of coordination is formation of the bridge 1 : 1 complexes of the a,a'-bipyridinyl type.

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17.
Инвентарный номер: нет.
   
   P 49

    Pestov, A. V.
    Synthesis in a gel as a new procedure for preparing carboxyethyl chitosan [Electronic resource] / A. V. Pestov, N. A. Zhuravlev, Yu. G. Yatluk // Russian Journal of Applied Chemistry. - 2007. - Vol. 80, № 7. - P1154-1159. - Bibliogr. : p. 1159 (14 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: A fundamentally new procedure of synthesis of carboxyethyl chitosan in a physical gel, ensuring higher degree of substitution at lower temperatures and lower consumption of time and chemicals, compared to the existing procedures, was developed. The structure of the resulting products was examined by diffuse reflection IR and 1H NMR spectroscopy in solutions and also 1H and 7Li broad line NMR

\\\\Expert2\\nbo\\Russian Journal of Applied Chemistry\\2007, v. 80, N. 7, p.1154.pdf
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18.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis in a gel and sorption properties of N-2-sulfoethyl chitosan / A. V. Pestov, Yu. S. Petrova, A. V. Bukharova, L. K. Neudachina, O. V. Koryakova, E. G. Matochkina, M. I. Kodess, Yu. G. Yatluk // Russian Journal of Applied Chemistry. - 2013. - Vol.86, №2. - С. 269-272. - Библиогр.: с. 272 (24 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CHELATES -- AMINO-CONTAINING POLYMER -- N-2-SULFOETHYL CHITOSAN
Аннотация: A new procedure was developed for preparation of chelate amino-containing polymer N-2-sulfoethyl chitosan by synthesis in a gel through the reaction between chitosan and sodium 2-bromoethanesulfonate, yielding a polymer with the degree of substitution of up to 0.5. The structure of the resulting polymers was confirmed by 1H NMR spectroscopy. The sorption characteristics with respect to transition and alkaline-earth metal ions were determined for the cross-linked polymers

\\\\expert2\\NBO\\Russian Journal of Applied Chemistry\\2013, v. 86, N 2, p.269.pdf
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19.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis and surface structural characteristics of new polysiloxane xerogel [Electronic resource] / A. S. Zasuhin, L. K. Neudachina, Yu. G. Yatluk, L. V. Adamova, O. A. Osipova, E. M. Gorbunova, Yu. S. Moskaleva, T. Yu. Lapina // Russian Journal of Physical Chemistry A, Focus on Chemistry. - 2011. - Vol. 85, № 3. - P478-482 : ил. - Bibliogr. : p. 482 (24 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Pyridylethylaminopropylpolysiloxane xerogel (PEAPPSX) was synthesized by sol-gel technology. The composition of the substance was determined via elemental analysis and 1H NMR spectroscopy. The surface structural characteristics of the xerogel were determined by electron microscopy and low-temperature nitrogen sorption; thermal analysis was also performed. It was established that the content of functional groups in PEAPPSX was 2.43 mmol/g, and that xerogel is a mesoporous substance with a developed surface (121.71 m(2)/g)

\\\\Expert2\\nbo\\Russian Journal of Physical Chemistry A, Focus on Chemistry\\2011, V.85, N 3, p.478.pdf
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20.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis and structure of the disc-like cluster C72H 102N12Ni13O40 [Электронный ресурс] / A. V. Pestov, P. A. Slepukhin, A. E. Permyakov, Yu. G. Yatluk // Journal of Structural Chemistry. - 2012. - Vol.53, №6. - P1017-1023
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
DISC-LIKE CLUSTER Ni13 -- SYNTHESIS -- METHYLIMINODIPROPIONIC ACID
Аннотация: The disc-like cluster C72H102N12Ni 13O40 is first time synthesized based on N-(2-pyridyl)methyliminodipropionic acid. Single crystal X-ray diffraction is used to determine its atomic structure. The cluster consists of seven-nuclear core: nickel(II) hydrocomplex (Ni.Ni distance 3.012-3.032 Å) and six nickel chelates of the corresponding acid arranged around its perimeter (Ni.Ni distance 2.981-3.164 Å). In the chelate part of the complex, the ligand is pentadentate owing to the formation of a bridging bond, thus organizing a coordination geometry of the metal center as a distorted square bipyramid (4+2). Liquid chromatography-mass spectrometry is employed to study the structure of the obtained nickel(II) complexes

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