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1.
Инвентарный номер: нет.
   
   S 98


   
    Synthesis and the molecular and crystal structures of methyl 2-substituted 7,7-dimethyl-5-oxo-5,6,7,8-tetrahydroquinoline-4-carboxylates [Electronic resource] / D. A. Rudenko, M. V. Artemova, P. A. Slepukhin, V. I. Karmanov, S. N. Shurov // Chemistry of Heterocyclic Compounds. - 2013. - Vol.48, №9. - P1321-1324
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SYNTHESIS -- MOLECULAR STRUCTURE -- CRYSTAL STRUCTURE
Аннотация: Methyl 7,7-dimethyl-5-oxo-5,6,7,8-tetrahydroquinoline-4-carboxylates were obtained as a result of 3-amino-5,5-dimethylcyclohex-2-enone reaction with the methyl esters of acyl(aroyl)pyruvic acids. The structure of methyl 7,7-dimethyl-5-oxo-2-phenyl-5,6,7,8-tetrahydroquinoline-4-carboxylate was established by X-ray structural analysis

\\\\Expert2\\NBO\\Chemistry of Heterocyclic Compounds\\2013, v.48, N 9, p. 1321-1324.pdf
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2.
Инвентарный номер: нет.
   
   O-97


   
    Oxidation of 1-methyl-1H-imidazole-2-thiol with chlorine dioxide [] / O. M. Lezina, S. A. Rubtsova, D. V. Belykh, P. A. Slepukhin, A. V. Kutchin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2013. - Vol.49, №1. - С. 112-118
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CHLORINE DIOXIDE -- OXIDATION CONDITIONS -- IMIDAZOLIUM CHLORIDE
Аннотация: Oxidation of 1-methyl-1H-imidazole-2-thiol with chlorine dioxide was performed for the first time, and the results were shown to depend on the oxidation conditions. Optimal conditions were found for the preparation of 1-methylimidazole-2-sulfonic acid, 2,2′-disulfanediylbis(1-methylimidazole) hydrochlorite, and 1-methyl-3-sulfo-3H-imidazolium chloride. A new salt, 4-methylanilinium 1-methyl-1H-imidazole-2-sulfonate, was isolated

\\\\Expert2\\NBO\\Russian Journal of Organic Chemistry\\2013, 49, (1), 112-118.pdf
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3.
Инвентарный номер: нет.
   
   S 98


   
    Synthesis of 5-substituted 8,8-dimethyl-8,9-dihydro-3H,7H-[1,2]oxazino[5,4,3-de]quinolin-3-ones [Electronic resource] / D. A. Rudenko, P. A. Slepukhin, V. I. Karmanov, M. I. Vakhrin, S. N. Shurov, Yu. A. Shchurov // Chemistry of Heterocyclic Compounds. - 2013. - Vol.48, №10. - 1539-1544.
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
HYDROXYLAMINE -- QUANTUM-CHEMICAL CALCULATIONS -- TETRAHYDROQUINOLINE-4-CARBOXYLIC ACIDS
Аннотация: The reaction of 2-substituted 7,7-dimethyl-5-oxo-5,6,7,8-tetrahydroquinoline-4-carboxylic acids with hydroxylamine results in the formation of 5-substituted 8,8-dimethyl-8,9-dihydro-3H,7H-[1,2]ox-azino[5,4,3-de]quinolin-3-ones. The structure of the 5-phenyl derivative has been established by X-ray structural analysis. A possible mechanism of the reaction has been proposed on the basis of nonempirical quantum-chemical calculations

\\\\Expert2\\NBO\\Chemistry of Heterocyclic Compounds\\2013, v.48, N 10, p. 1539-1544.pdf
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4.
Инвентарный номер: нет.
   
   S 98


   
    Synthesis of novel fluorine- and iodine-containing [1,2,4]triazolo[3,4-b][1,3]thiazines based 3-(alkenylthio)-5-(trifluoromethyl)-4H-1,2,4-triazole-3-thiols [Electronic resource] / E. S. Ilinykh, D. G. Kim, M. I. Kodess, E. G. Matochkina, P. A. Slepukhin // Journal of Fluorine Chemistry. - 2013. - Vol.149. - P24-29
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SYNTHESIS -- FLUORINE-CONTAINING -- IODIDES
Аннотация: In this paper we report the synthesis of novel S-alkenyl derivatives of 5-(trifluoromethyl)-4H-1,2,4-triazole-3-thiol via alkenation reaction with different alkenyl halides. Reaction between the resulting S-alkenation products and iodine proceeds regiospecifically to give new fused fluorine- and iodine-containing [1,2,4]triazolo[3,4-b][1,3]thiazine heterocyclic systems. The structure of synthesized compounds was confirmed by mass spectra, IR, 1H, 13C and 19F NMR spectroscopy including 2D 1H–13C HSQC, 1H–1H COSY, 1H–13C HMBC correlations, elemental analysis and single-crystal X-ray diffraction study. --------------------------------------------------------------------------------

\\\\Expert2\\NBO\\Journal of Fluorine Chemistry\\2013, v. 149, p.24.pdf
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5.
Инвентарный номер: нет.
   
   S 98


   
    Synthesis of 7-cycloalkylimino substituted 3-amino-6-fluoro-2-methyl-3H-quinazolin-4-ones [Electronic resource] / E. V. Nosova, G. N. Lipunova, P. A. Slepukhin, V. N. Charushin // Journal of Fluorine Chemistry. - 2013. - Vol.145. - P63-65
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SYNTHESIS -- NUCLEOPHILIC SUBSTITUTION -- X-RAY ANALYSIS
Аннотация: A versatile pathway for the synthesis of 7-cycloalkylimino substituted 3-amino-6-fluoro-2-methyl-3H-quinazolin-4-ones from 4,5-difluoroanthranylic acid has been advanced. Nucleophilic amination–defluorination reaction of the 6,7-difluoro derivative of 3-amino-2-methyl-3H-quinazolin-4-one has been established to occur at position 7, as shown by X-ray crystallographic analysis. --------------------------------------------------------------------------------

\\\\Expert2\\NBO\\Journal of Fluorine Chemistry\\2013, v. 145, p.63.pdf
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6.
Инвентарный номер: нет.
   
   T 82


   
    Trans-Dichlorobis{(1R,4S)-1,7,7-trimethyl-3-[(S)-α-methylbenzylimino]bicyclo[2.2.1]heptan-2-one-N}Palladium(II): Synthesis and structural examination [Electronic resource] / O. A. Zalevskaya, O. A. Gur'eva, L. L. Frolova, I. N. Alekseev, P. A. Slepukhin, A. V. Kuchin // Russian Journal of Coordination Chemistry. - 2013. - Vol.39, №1. - P37-40
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
PALLADIUM(II) -- SYNTHESIS -- STRUCTURAL EXAMINATION
Аннотация: A reaction of (1R,4S)-1,7,7-trimethyl-3-[(S)-α-methylbenzylimino]bicyclo[2.2.1]heptan-2-one with lithium tetrachloropalladate gave a chiral palladium(II) complex with monodentate coordination of the organic ligand. The structure of the complex was confirmed by NMR spectra and X-ray diffraction data

\\\\Expert2\\NBO\\Russian Journal of Coordination Chemistry\\2013, v. 39, N. 1, p.37.pdf
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7.
Инвентарный номер: нет.
   
   S 98


   
    Synthesis and reduction of new sulfinimines with isobornane structure [Electronic resource] / E. S. Izmest’ev, D. V. Sudarikov, S. A. Rubtsova, P. A. Slepukhin, A. V. Kuchin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2012. - Vol.48, №11. - P1407-1418
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SULFINIMINES -- SYNTHESIS -- ISOBORNANETHIOL
Аннотация: Synthesis of sulfenimines proceeding from isobornanethiol with yields up to 78% was performed. They were oxidized to diastereomeric isobornylsulfinimines and the latter were reduced to N-substituted isobornylsulfinamides in high yields

\\\\Expert2\\NBO\\Russian Journal of Organic Chemistry\\2012, 48 (11), 1407-1418.pdf
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8.
Инвентарный номер: нет.
   
   F 62


   
    Five-membered 2,3-dioxoheterocycles: XC. Reaction of 4,5-bis(methoxycarbonyl)-1H-pyrrole-2,3-diones with enaminoesters. crystal and molecular structure of 4-methyl 9-ethyl 7-benzyl-3-hydroxy-8-methyl-1-(4-methoxyphenyl)-2,6-dioxo-1,7-diazaspiro[4.4]nona-3,8-diene-4,9-dicarboxylate [Electronic resource] / P. S. Silaichev, M. A. Chudinova, P. A. Slepukhin, A. N. Maslivets // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2012. - Vol.48, №11. - P1435-1438
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
DICARBOXYLATES -- METHOXYPHENYL -- BENZYLAMINO
Аннотация: 1-Aryl-4,5-bis(methoxycarbonyl)-1H-pyrrole-2,3-diones react with ethyl 3-(benzylamino)but-2-enoate and ethyl 3-(benzylamino)-3-phenylacrylate giving 4-methyl 9-ethyl 1-aryl-7-benzyl-3-hydroxy-8-methyl- and 4-methyl 9-ethyl 1-aryl-7-benzyl-3-hydroxy-8-phenyl-2,6-dioxo-1,7-diazaspiro[4.4]nona-3,8-diene-4,9-dicarboxylates

\\\\Expert2\\NBO\\Russian Journal of Organic Chemistry\\2012, 48 (11), 1435-1438.pdf
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9.
Инвентарный номер: нет.
   
   P 49


    Pestov, A. V.
    Comparative coordination ability of N-(2-hydroxyethyl)aminoacetic acid and O-(2-hydroxyethyl)hydroxyacetic acid in the copper(II) complexes [Electronic resource] / A. V. Pestov, P. A. Slepukhin, Yu. G. Yatluk // Russian Journal of Coordination Chemistry. - 2012. - Vol.38, №12. - P738-743
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
COPPER(II) -- N-(2-HYDROXYETHYL)AMINOACETIC -- O-(2-HYDROXYETHYL)HYDROXYACETIC ACIDS
Аннотация: Copper(II) complexes based on N-(2-hydroxyethyl)aminoacetic and O-(2-hydroxyethyl)hydroxyacetic acids were synthesized. Their structures were studied by X-ray diffraction analysis. The coordination spheres of the copper metal center were compared in the condensed phase for the both ligands

\\\\Expert2\\NBO\\Russian Journal of Coordination Chemistry\\2012, v. 38, N. 12, p.738.pdf
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10.
Инвентарный номер: нет.
   
   S 98


   
    Synthesis, structure and complexation of the fluorinated 1,3-enaminoketones containing at the nitrogen atom substituents with a terminal C≡C bond [Electronic resource] / E. F. Zhilina, P. A. Slepukhin, N. S. Boltacheva, M. G. Pervova, D. L. Chizhov, V. I. Filyakova, V. N. Charushin // Russian Journal of General Chemistry. - 2012. - Vol. 82, №12. - P1962-1969
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SYNTHESIS -- NITROGEN -- TERMINAL C≡C BONDS
Аннотация: The reaction of fluorinated lithium 1,3-diketonates with propargylamine hydrochloride and 1,1,1-trifluorpentane-2,4-dione or 1,1,1-trifluoro-4-methoxypent-3-en-2-one with propargylamine and 3-aminophenylacetylene were performed to obtain fluorinated 1,3-enaminones containing at a nitrogen atom substituents with terminal C≡C bonds: (Z)-1,1,1-trifluoro-4-(2-propynylamino)-3-pentene-2-one, (Z)-1,1,2,2-tetrafluoro-5-(2-propynylamino)-4-hexen-3-one, and 4-(3-ethynylphenylamino)-1,1,1-trifluoropentyl-3-en-2-one. Reactions of 4-(3-ethynyl-phenylamino)-1,1,1-trifluoro-pentyl-3-en-2-one with Cu(II) acetate or nanosized powder of copper or its oxides led to the respective chelate complex. The structure of (Z)-1,1,2,2-tetrafluoro-5-(2-propynylamino)-4-hexen-3-one and a copper complex of 4-(3-etinilphenylamino)-1,1,1-trifluoropenta-3-en-2-one was determined by XRD

\\\\Expert2\\NBO\\Russian Journal of General Chemistry\\2012, V. 82, N 12, p. 1962–1969.pdf
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11.
Инвентарный номер: нет.
   
   V 50


    Vershinina, E. A.
    Synthesis of oxazolo[3,2-a]quinolinium triiodide from 4-methyl-1-(3-methylbut-2-enyl)quinolin-2(1H)-one [Electronic resource] / E. A. Vershinina, P. A. Slepukhin, D. G. Kim // Chemistry of Heterocyclic Compounds. - 2012. - Vol.47, №12. - P1596-1597
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SYNTHESIS -- TRIIODIDE -- QUINOLINE

\\\\Expert2\\NBO\\Chemistry of Heterocyclic Compounds\\2011, v.47, N 12, p.1596-1597.pdf
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12.
Инвентарный номер: нет.
   
   F 76


   
    Formation of 4-aroylhydrazono-2-methyl- 5-oxo-1-phenyl-3-phenylaminooxalyl-pyrrolidine-2-carboxylates [Electronic resource] / V. L. Gein, R. O. Dyrenkov, N. A. Kornienko, M. I. Vakhrin, G. A. Veikhman, P. A. Slepukhin // Chemistry of Heterocyclic Compounds. - 2012. - Vol.47, №12. - P1590-1592
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
PHENYLAMINOOXALYL -- PYRROLIDINE -- CARBOXYLATES

\\\\Expert2\\NBO\\Chemistry of Heterocyclic Compounds\\2011, v.47, N 12, p.1590-1592.pdf
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13.
Инвентарный номер: нет.
   
   I-70


   
    Investigation of the structure of chitosan hybrid systems by pH-sensitive nitroxyl radical [Electronic resource] / A. V. Mekhaev, A. V. Pestov, L. S. Molochnikov, E. G. Kovaleva, Yu. G. Yatluk, I. A. Grigor'ev, I. A. Kirilyuk // Russian Journal of Physical Chemistry A, Focus on Chemistry. - 2011. - Vol. 85, № 6. - P987-992. - Bibliogr. : p. 991-992 (24 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Hybrid organo-inorganic materials based on the chitosan-SiO2, chitosan-Al2O3, and chitosancellulose systems are prepared. The structure of the surface is studied by means of EPR spectroscopy using the stable pH-sensitive nitroxyl radical, 4-dimethylamino-2-ethyl-5,5-dimethyl-2-pyridine-4-yl-2,5-dihydro-1H-imidazole-1-oxyl as adsorbed probe molecules, and the processes that occur during the formation of hybrid materials are considered

\\\\Expert2\\nbo\\Russian Journal of Physical Chemistry A, Focus on Chemistry\\2011, V.85, N 6, p.987.pdf
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14.
Инвентарный номер: нет.
   
   N 10


   
    N-2-(2-pyridyl)ethyl chitosan: Synthesis in gel and sorption properties [Electronic resource] / A. V. Pestov, S. YU. Bratskaya, Yu. A. Azarova, M. I. Kodess, Yu. G. Yatluk // Russian Journal of Applied Chemistry. - 2011. - Vol. 84, № 4. - P713-718 : рис., табл. - Bibliogr. : p. 717-718 (16 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: A procedure was developed for preparing a new heterocyclically substituted chelating aminopolymer, N-2-(2-pyridyl)ethyl chitosan, by direct addition of 2-vinylpyridine to chitosan under the conditions of synthesis in gel. The resulting polymer has the degree of substitution of up to 1. The ability of the samples obtained to sorb transition and noble metal ions was evaluated

\\\\Expert2\\nbo\\Russian Journal of Applied Chemistry\\2011, v. 84, N 4, p.713.pdf
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15.
Инвентарный номер: нет.
   
   X 10


   
    X-ray diffraction study of 1,5-bis-(4',4',4'-trifluoro-1'-methyl-3'-oxo-but-1'-enylamino)-3-oxapentane [Electronic resource] / P. A. Slepukhin, N. S. Boltacheva, V. I. Filyakova, V. N. Charushin // Journal of Structural Chemistry. - 2011. - Vol. 52, № 2. - P443-444. - Bibliogr. : p. 444 (3 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Specific features of the molecular and crystal structures of 1,5-bis-(4?,4?,4?-trifluoro-1?-methyl-3?-oxo-but-1?-enylamino)-3-oxapentane are determined by single crystal XRD

\\\\Expert2\\nbo\\Journal of Structural Chemistry\\2011, V. 52, N 2, p.443-444.pdf
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16.
Инвентарный номер: нет.
   
   S 98


   
    Synthesis, structure, tuberculostatic activity, and toxicity of fluoroalkyl-containing 3-hydroxyimino-1,5-benzodiazepines [Electronic resource] / O. G. Khudina, Ya. V. Burgart, M. A. Kravchenko, V. I. Saloutin // Pharmaceutical Chemistry Journal. - 2011. - Vol. 45, № 2. - P75-78. - Bibliogr. : p. 78 (11 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: An improved method for the synthesis of fluoroalkyl-containing 3-hydroxyimino-1,5-benzodiazepines is proposed. For this, 3-hydroxyimines were obtained via nitrosation of 1,3-diketones and 3-oxoesters by tert-butylnitrite in diethylether under acid catalysis conditions and were reacted without isolation and further purification with ortho-phenylenediamine. It was found that polyfluoroalkyl-containing 3-hydroxyimino-1,5-benzodiazepin-2-ones and 2-hydroxy-3-hydroxyimino-2-trifluoromethyl-4-phenyl-1H-1,5-benzodiazepine possess high tuberculostatic activity comparable with that of isoniazide. Tests for acute toxicity of the trifluoromethylated heterocycles showed that they are less toxic than isoniazide

\\\\Expert2\\nbo\\Pharmaceutical Chemistry Journal\\2011, 45 (2), 75.pdf
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17.
Инвентарный номер: нет.
   
   S 98


   
    Synthesis of 6,7-dihydro-5H-[1,3,4]thiadiazolo-[2,3-b][1,3]thiazinium system derivatives [Electronic resource] / D. G. Kim, N. M. Sudolova, P. A. Slepukhin, V. N. Charushin // Chemistry of Heterocyclic Compounds. - 2011. - Vol. 46, № 11. - P1420-1421. - Bibliogr. : p. 1421 (3 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

\\\\Expert2\\nbo\\Chemistry of Heterocyclic Compounds\\2011, v.46, N 11, p.1420-1421.pdf
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18.
Инвентарный номер: нет.
   
   S 98


   
    Synthesis and photophysical properties of 2-styrylquinazolin-4-ones [Electronic resource] / T. V. Trashakhova, E. V. Nosova, M. S. Valova, P. A. Slepukhin, G. N. Lipunova, V. N. Charushin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2011. - Vol. 47, № 5. - P753-761. - Bibliogr. : p. 761 (16 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: trans-2-Styryl-substituted 3H-, 3-phenyl-, and 3-naphthylquinazolin-4-ones and their 6,7-difluoro derivatives were synthesized by condensation of appropriate 2-methylquinazolin-4-ones with aromatic aldehydes or by the transformation of the heterocycle of 2-methyl-3,1-benzoxazin-4-one under the action of benzylidenephenylamines

\\\\Expert2\\nbo\\Russian Journal of Organic Chemistry\\2011, 47 (5), 753-761.pdf
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19.
Инвентарный номер: нет.
   
   N 52


   
    New chiral metal complexes based on 2-ethoxymethylidene-3-oxo-3-polyfluoroalkylpropionates [Electronic resource] / Yu. S. Kudyakova, M. V. Goryaeva, Ya. V. Burgart, V. I. Saloutin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2011. - Vol. 47, № 3. - P331-339. - Bibliogr. : p. 339 (10 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Ethyl 2-ethoxymethylidene-3-oxo-3-polyfluoroalkylpropionates reacted with (1S,2S)-1,2-diphenylethane-1,2-diamine to give diethyl 2,2?-{[(1S,2S)-diphenylethane-1,2-diyl]bis[iminomethylidene]}bis(3-oxo-3-polyfluoroalkyl)alkanoates which were used as ligands to obtain chiral complexes with transition metals ??

\\\\Expert2\\nbo\\Russian Journal of Organic Chemistry\\2011, 47 (3), 331-339.pdf
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20.
Инвентарный номер: нет.
   
   R 30


   
    Reactions of 3-aminoisoxazolo[4,5-c]coumarin with benzoyl chloride: the first example of a preparative 1,2,4-oxadiazole–oxazole rearrangement [Electronic resource] / V. Ya. Sosnovskikh, V. S. Moshkin, M. Yu. Kornev, M. I. Kodess // Mendeleev Communications. - 2011. - Vol. 21, № 2. - P110-111. - Bibliogr. : p. 111 (7 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Depending on conditions, reaction of 3-amino-4H-chromeno[3,4-d]isoxazol-4-one with benzoyl chloride gives 4-hydroxy- and/or 4-benzoyloxy-3-(5-phenyl-1,2,4-oxadiazol-3-yl)coumarins, which are rearranged into 2-benzamido-4H-chromeno[3,4-d]oxazol-4-one by heating in DMSO

\\\\Expert2\\nbo\\Mendeleev Communications\\2011, v.21, p.110.pdf
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Сиглы отделов ЦНБ УрО РАН


  бр.ф. - Бронированный фонд

  бф - Научно-библиографический отдел

  БХЛ - Фонд художественной литературы

  ИИиА -Фонд исторической литературы в ЦНБ УрО РАН

  ИМЕТ -Отдел ЦНБ в Институте металлургии УрО РАН

  кх - Отдел фондов (книгохранениe)

  МБА - Межбиблиотечный абонемент

  мф - Методический фонд

  ок - Отдел научной каталогизации

  оку - Отдел комплектования и учета

  орф - Обменно-резервный фонд

  пф - Читальный зал деловой и патентной информации

  рк - Фонд редкой книги

  ч/з - Главный читальный зал

  эр - Зал электронных ресурсов

  

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