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Труды сотрудников Института органического синтеза УрО РАН - результаты поиска

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Каталог книг и продолжающихся изданий
Сводный каталог иностранных периодических изданий, имеющихся в библиотеках УрО РАН
Сводный каталог отечественных периодических изданий, имеющихся в библиотеках УрО РАН
Каталог диссертаций и авторефератов диссертаций УрО РАН
Каталог препринтов УрО РАН (1975 г. - )
Имидж-каталог отечественных книг (до 2010 г.)
Имидж-каталог иностранных книг (до 2010 г.)
Алфавитно-предметный указатель (АПУ) ЦНБ УрО РАН
Публикации об УрО РАН
Изобретения уральских ученых
Интеллектуальная собственность (статьи из периодики)
Нанотехнологии
Демидовские премии
Гибель династии Романовых
История Урала
Личная библиотека С. В. Вонсовского
Книжная коллекция Шубиных
Труды Института высокотемпературной электрохимии УрО РАН
Труды Института истории и археологии УрО РАН
Труды сотрудников Института горного дела УрО РАН
Труды сотрудников Института органического синтеза УрО РАН
Труды сотрудников Института теплофизики УрО РАН
Труды сотрудников Института химии твердого тела УрО РАН
Расплавы
Труды сотрудников ЦНБ УрО РАН
Публикации Черешнева В.А.
Публикации Чарушина В.Н.
Каталог библиотеки ИЭРиЖ УрО РАН
Электронная энциклопедия «Дискурсология»
Библиометрия
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1.
Инвентарный номер: нет.
   
   С 38

   
    Синтез фторсодержащих аналогов эллиптицина и других гетероциклов на омнове 2-нитро- и 2-амино-4.5-дифторанилинов [] = Synthesis of fluorine-containing analogs of ellipticine and other heterocycles from 2-nitro- and 2-amino-4,5-difluoroanilines / В. Н. Яровенко, А. В. Полушина, К. С. Левченко, И. В. Заварзин, М. М. Краюшкин, С. К. Котовская, В. Н. Чарушин // Журнал органической химии. - 2007. - Т. 43, Вып. 9. - С. 1391-1396 : рис., табл. - Библиогр. : с. 1396 (12 назв.) . - ISSN 0514-7492
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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2.
Инвентарный номер: нет.
   

   
    The synthesis of aminophenyl-substituted 2,2′-bipyridine ligands by “1,2,4-triazine” methodology / A. P. Krinochkin, D. S. Kopchuk, M. I. Savchuk [et al.] // AIP Conference Proceedings. - 2021. - Vol. 2388, № 1. - Ст. 030016
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: A convenient synthetic approach to the 2,2’-bipyridines, including those with a condensed cyclopentene fragment, having an aminophenyl substituent at the C5 or C6 positions is reported. The products were obtained via their 1,2,4-triazine analogs with a nitro group, by the subsequent transformation of their 1,2,4-triazine ring into a pyridine one and the reduction of the nitro group to the amino group.

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3.
Инвентарный номер: нет.
   
   T 44

   
    The N1-glycoside analogs of 6-azacytidine. Cytotoxic effect and influence on transcription in vitro [Text] / L. G. Pal'chikovs'ka, L. V. Garmanchuk, I. V. Alekseeva, L. S. Usenko, T. S. Shestakova, G. I. Solyanik, A. D. Shved, V. F. Chekhun // Biopolimeri i Klitina. - 2005. - Vol. 21, № 5. - P433-439
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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4.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis of novel 3-(pyridin-4-yl)-1,2,4-triazines, their analogs and study of the activity against vaccinia virus / O. V. Shabunina, Y. K. Shtaitz, D. S. Kopchuk [et al.] // Chemistry of Heterocyclic Compounds. - 2021. - Vol. 57, № 4. - P462–466
УДК
Г
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
1,2,4-TRIAZINES -- ANTIVIRAL ACTIVITY -- IPSO SUBSTITUTION -- NUCLEOPHILIC HYDROGEN SUBSTITUTION
Аннотация: Using atom-economical approaches, new representatives of 3-(pyridin-4-yl)-1,2,4-triazines and their 4-nitrophenyl analogs were obtained, and their activity in relation to the vaccinia virus was studied. The new compounds have shown promising characteristics, in particular, in comparison to the antiviral drug Cidofovir.

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5.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis of fluorine-containing analogs of ellipticine and other heterocycles from 2-Nitro-and 2-amino-4,5-difluoroanilines [Electronic resource] / V. N. Yarovenko, A. V. Polushina, K. S. Levchenko, I. V. Zavarzin, M. M. Krayushkin, S. K. Kotovskaya, V. N. Charushin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2007. - Vol. 43, № 9. - P1387-1392
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: 2-Nitro- and 2-amino-4,5-difluoroanilines were used as starting materials to synthesize fluorine-containing imidazole, oxazole, and indoloquinoxaline derivatives. The latter may be regarded as ellipticine analogs

\\\\Expert2\\nbo\\Russian Journal of Organic Chemistry\\2007, 43 (9), 1387.pdf
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6.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis of 5-trifluoromethylpyrazol-1-yl-substituted 1,2,4,5-tetrazines [Electronic resource] / S. G. Tolshchina, N. K. Ignatenko, P. A. Slepukhin, R. I. Ishmetova, G. L. Rusinov // Chemistry of Heterocyclic Compounds. - 2010. - Vol. 46, № 6. - P691-698 : рис., табл.
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
5-HYDROXY-5-TRIFLUOROMETHYLPYRAZOLINES -- 1,2,4,5-TETRAZINES -- 1,1,1-TRIFLUORO-2,4-PENTANEDIONE
Аннотация: Previously unknown products of the cyclocondensation of 1,1,1-trifluoro-2,4-pentanedione with triaminoguanidine and hydrazine derivatives of 1,2,4,5-tetrazine have been obtained. 5-Hydroxy-5-trifluoromethylpyrazoline substituents formed on the tetrazine ring were dehydrated under the action of trifluoroacetic anhydride. A comparison has been carried out of the reactivity of 5-trifluoromethylpyrazolyl-substituted 1,2,4,5-tetrazines and their unfluorinated analogs in nucleophilic substitution and [4 + 2] cycloaddition reactions

\\\\Expert2\\nbo\\Chemistry of Heterocyclic Compounds\\2010, v.46, N 6, p.691-698.pdf
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7.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis of 5-and 7-fluoroquinazolin-4(1H)-ones [Electronic resource] / A. A. Layeva, E. V. Nosova, G. N. Lipunova, T. V. Trashakhova, V. N. Charushin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2007. - Vol. 56, № 9. - P1821-1827
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: 5-Fluoroquinazoline-2,4-diones and their 2-thio analogs were obtained from 6-fluoroanthranilic acid. Two convenient routes to 5-fluoroquinazolin-4-ones involved cyclocondensation of 6-fluoroanthranilamide with acid chlorides (anhydrides) or with aromatic (heterocyclic) aldehydes. A method for the synthesis of 7-fluoroquinazolin-4-one from 2,4-difluorobenzoic acid was proposed

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2007, 56 (9), 1821.pdf
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8.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis and properties of heterocycle-containing podands / E. S. Filatova, O. V. Fedorova, G. L. Rusinov, O. N. Charushin // Chemistry of Heterocyclic Compounds. - 2021. - Vol. 57, № 10. - P971–983
УДК
54
ББК Г
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
HETEROCYCLE-CONTAINING PODANDS -- GLYCOL -- OLIGO(OXYETHYLENE) SPACER -- OPEN-CHAIN ANALOGS OF CROWN ETHERS
Аннотация: The review is devoted to noncyclic analogs of crown ethers (podands) containing an oxyethylene spacer and heterocyclic fragments at one or both of its ends. The paper considers publications on the methods of obtaining and properties of podands for the 2010–2021 period.

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9.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis and GC-MS study of fluorinated esters derived from thrimethylolpropane [Electronic resource] / M. G. Pervova, V. E. Kirichenko, T. I. Gorbunova, A. Ya. Zapevalov, V. I. Saloutin // Russian Journal of General Chemistry. - 2008. - Vol. 78, № 9. - P1701-1706
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Zol-gel process was used to synthesize equilibrium mixtures of mono-, di-, and trimester derived from trimethylolpropane and perfluorocarboxylic acids. The elution order of the components of the mixtures from a weakly polar HP-5 column was established. The mass spectra of the synthesized compounds were studied. The GC-MS parameters of the products were compared with the respective parameters of their nonfluorinated analogs. The characteristics of the fluorinated esters have features determined by the esterification degree and the nature of the perfluoroalkyl groups, due to which these compounds can be identified in mixtures

\\\\Expert2\\nbo\\Russian Journal of General Chemistry\\2008, V. 78, N 9, p.1701.pdf
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10.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis and antiviral activity of nucleoside analogs based on 1,2,4-triazolo[3,2-c][1,2,4]triazin-7-ones [Electronic resource] / V. L. Rusinov, O. N. Chupakhin, S. L. Deev, T. S. Shestakova, E. N. Ulomskii, L. I. Rusinova, O. I. Kiselev, E. G. Deeva // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2010. - Vol. 59, № 1. - P136-143
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
NUCLEOSIDE ANALOGS -- ANTIVIRAL DRUGS -- HYDROXYETHOXYMETHYL
Аннотация: Nucleoside analogs containing hydroxybutyl, hydroxyethoxymethyl, allyloxymethyl, and propargyloxymethyl fragments were synthesized based on 1,2,4-triazolo[3,2-c][1,2,4]triazin-7-ones isosteric to purine bases. Some of the compounds obtained inhibit in vitro reproduction of influenza and respiratory syncytial virus infection

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2010, 59 (1), 136-143.pdf
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11.
Инвентарный номер: нет.
   

   
    Synthesis and antioxidant activity of new neomenthyl and caranyl thiotriazoles / Y. V. Gyrdymova, D. V. Sudarikov, S. A. Rubtsova, S. A. Patov, A. V. Kuchin, O. G. Shevchenko, P. A. Slepukhin, F. A. Lakhvich, F. S. Pashkovskii // Chemistry of natural compounds. - 2018. - Vol. 54, № 5. - P883-888
Кл.слова (ненормированные):
TRIAZOLES -- NEOMENTHANE AND CARANE SULFIDES
Аннотация: New neomenthyl and caranyl thiotriazoles were synthesized in up to 80% yields. Studies of the antioxidant and membrane-protective activity of the synthesized compounds in vitro showed that sulfides with a carane moiety were more active than analogs with a neomenthane substituent.

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12.
Инвентарный номер: нет.
   
   R 30

   
    Steric structure of alkyl 2-aryl(hetaryl)hydrazono-3-fluoroalkyl-3-oxopropionates [Electronic resource] / E. V. Shchegol'kov, Ya. V. Burgart, O. G. Khudina, V. I. Saloutin, O. N. Kazheva, A. N. Chekhlov // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2009. - Vol. 45, № 6. - P801-809
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Steric structure of fluorinated 2-arylhydrazono-3-oxo esters was studied by 1H, 19F, and 13C NMR spectroscopy and X-ray analysis. It was found that these compounds in the crystalline state and in solutions in acetone-d 6, DMSO-d 6, and CDCl3 exist as Z isomers with the ester fragment involved in intramolecular hydrogen bond with the hydrazone NH proton. Exceptions are alkyl 2-arylhydrazono-4,4-difluoro-3-oxobutanoates which exist in acetone-d 6 as mixtures of Z and E isomers, the former prevailing. Unlike fluorinated analogs, ethyl 2-(4-methylphenyl)hydrazono-3-oxobutanoate in crystal has the structure of E isomer in which intramolecular hydrogen bond is formed between the NH proton and acetyl carbonyl group. The same compound in acetone-d 6, DMSO-d 6, and CDCl3 gives rise to a mixture of Z and E isomers, the latter prevailing

\\\\Expert2\\nbo\\Russian Journal of Organic Chemistry\\2009, 45 (6), 801.pdf
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13.
Инвентарный номер: нет.
   
   S 83

   
    Stereochemical aspects in the synthesis of novel N-(purin-6-yl)dipeptides as potential antimycobacterial agents / V. V. Musiyak, I. A. Nizova, E. N. Chulakov [et al.] // Amino Acids. - 2021. - Vol. 53, № 3. - P407-415
ББК Г
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
DIPEPTIDES -- RACEMIZATION -- PURINE -- COUPLING -- NUCLEOPHILIC SUBSTITUTION -- ANTIMYCOBACTERIAL ACTIVITY
Аннотация: The synthesis of purine conjugates with natural amino acids is one of the promising directions in search for novel therapeutic agents, including antimycobacterial agents. The purpose of this study was to synthesize N-(purin-6-yl)dipeptides containing the terminal fragment of (S)-glutamic acid. To obtain the target compounds, two synthetic routes were tested. The first of them is based on coupling of N-(purin-6-yl)-(S)-amino acids to dimethyl (S)-glutamate in the presence of carbodiimide coupling agent followed by the removal of ester groups. However, it turned out that this coupling process was accompanied by racemization of the chiral center of N-(purin-6-yl)-α-amino acids and in all cases led to mixtures of (S,S)- and (R,S)diastereomers (6:4). Individual (S,S)-diastereomers were obtained using an alternative approach based on the nucleophilic substitution of chlorine in 6-chloropurine or 2-amino-6-chloropurine with corresponding dipeptides as nucleophiles. The enantiomeric purity of the target compounds was confirmed by chiral HPLC. To test the assumption that racemization of the chiral center of N-(purin-6-yl)-α-amino acids occurs with the participation of nitrogen atoms of the imidazole ring via the stage of formation of a chirally labile intermediate, we obtained such structural analogs of N-(purin-6-yl)-(S)-alanine as N-(9-benzylpurin-6-yl)-(S)-alanine and N-(7-deazapurin-6-yl)-(S)-alanine. It was found that coupling of these compounds to dimethyl (S)-glutamate was also accompanied by racemization. This indicates that the imidazole fragment does not play a crucial role in this process. When testing the antimycobacterial activity of some of the obtained compounds, conjugates with moderate activity against the laboratory Mycobacterium tuberculosis H37Rv strain (MIC 3.1–6.25 μg/mL) were identified.

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14.
Инвентарный номер: нет.
   
   S 78

   
    Spin-spin coupling constants 13C-15N and 1H-15N in the investigation of azido-tetrazole tautomerism in a series of 2-azidopyrimidines [Electronic resource] / I. A. Khalymbadzha, T. S. Sheshukova, S. L. Deev , V. L. Rusinov, O. N. Chupakhin, Z. O. Shenkarev, A. S. Arseniev // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2013. - Vol.62, №2. - С. 521-528. - Bibliogr. : p. 528 (25 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
AZIDO-TETRAZOLE EQUILIBRIUM -- SPIN-SPIN COUPLING -- 2-AZIDOPYRIMIDINES
Аннотация: A new method was developed for the investigation of an azido-tetrazole equilibrium based on using a complex analysis of 13C-15N and 1H-15N spin-spin coupling constants. The use of this approach became possible due to the selective inclusion of 15N isotopes into the structures of 2-azidopyrimidines and their cyclic analogs tetrazolo[1,5-a]pyrimidines

\\\\expert2\\nbo\\Russian Chemical Bulletin\\2013, 62 (2), 521-528.pdf
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15.
Инвентарный номер: нет.
   
   N 39

    Nemytov, A. I.
    SNH methodology in the synthesis of quinazolinap precursors and analogs / A. I. Nemytov, V. A. Ishkhanyan, I. A. Utepova, O. N. Chupakhin // Современные синтетические методологии для создания лекарственных препаратов и функциональных материалов (MOSM2018): вторая международная научно-практическая конференция : материалы и доклады. - Екатеринбург, 2019. - С. 138
ББК Г
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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16.
Инвентарный номер: нет.
   

   
    Single-crystal x-ray diffraction studies in a series of 5-pentafluorophenyl-2,2'-bipyridines and their fused analogs / M. V. Varaksin, E. S. Starnovskaya, D. S. Kopchuk [и др.] // Russian journal of general chemistry. - 2020. - Т. 90, № 2. - P235-237
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
6-ARYL-5-PENTAflUOROPHENYL-2,2'-BIPYRIDINES -- LIGANDS -- SINGLE-CRYSTAL X-RAY DIFFRACTION ANALYSIS -- STRUCTURAL EFFECT
Аннотация: Structure of three 6-aryl-5-pentafluorophenyl-2,2'-bipyridines has been studied by means of single-crystal X-ray diffraction analysis. The effect of some functional fragments on the structural organization of compounds, in particular, donor and acceptor substituents in the aryl moiety, as well as annulated benzene and cyclopentane rings on the molecular structure and crystal packing of pentafluorophenyl-modified 2,2'-bipyridine ligand systems has been analyzed.

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17.
Инвентарный номер: нет.
   
   R 45

   
    Resistance of polyfluorinated complete esters of polyhydric alcohols to thermal oxidation: Comparison with nonfluorinated analogs [Electronic resource] / T. I. Gorbunova, S. M. Sorokina, A. Ya. Zapevalov, V. I. Saloutin // Russian Journal of General Chemistry. - 2006. - Vol. 76, № 11. - P1795-1800
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Complete esters of pentaerythritol, trimethylolpropane, and 2,2-dimethyl-1,3-propanediol with polyfluorinated carboxylic acids were prepared by esterification. As determined by differential thermal gravimetric analysis in air, the resistance of the esters to thermal oxidation decreases in going from pentaerythritol derivatives to those of trimethylolpropane and then to those of 2,2-dimethyl-1,3-propanediol. The compounds synthesized surpass their nonfluorinated analogs in the resistance to thermal oxidation.

\\\\Expert2\\nbo\\Russian Journal of General Chemistry\\2006, V. 76, N 11, p.1795.pdf
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18.
Инвентарный номер: нет.
   

   
    Polyfluoroalkylated antipyrines in Pd-catalyzed transformations / E. V. Shchegolkov, Y. V. Burgart, D. A. Matsneva [et al.] // RSC Advances. - 2021. - Vol. 11, № 56. - P35174-35181
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: In the direct C–H arylation with arylhalogenides in the presence of Pd(OAc)2, trifluoromethyl-containing antipyrine reacts very slowly and incompletely owing to the low nucleophilicity of its C4 center. However, it was effective in modifying polyfluoroalkyl-substituted 4-bromo- and 4-iodo antipyrines by the Suzuki and Sonogashira reactions. It was established that using Pd2(dba)3 as catalyst and XPhos as phosphine ligand was the optimal catalytic system for the synthesis of 4-aryl- and 4-phenylethynyl-3-polyfluoroalkyl-antipyrines. Moreover, iodo-derivatives as the initial reagents were found to be more advantageous compared to bromo-containing analogs. It was found that 4-phenylethynyl-5-CF3-antipyrine has a moderate activity against the influenza virus A/Puerto Rico/8/34 (H1N1) and 4-iodo-5-CF3-antipyrine reveals a weak activity against the vaccine virus (strain Copenhagen) and bovine diarrhea virus (strain VC-1).

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19.
Инвентарный номер: нет.
   
   N 52

   
    New approach to the synthesis of azauracils and azaisocytosines [Electronic resource] / T. S. Shestakova, S. L. Deev, E. N. Ulomskii, V. L. Rusinov, O. N. Chupakhin, O. A. Dyachenko, O. N. Kazheva, A. N. Chekhlov, P. A. Slepukhin, M. I. Kodess // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2006. - Vol. 55, № 11. - P2071-2080
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: A new procedure was developed for the synthesis of 6-phenyltetrazolo[1,5-b]triazin-7-one. Aza analogs of uracil and isocytosine were prepared by the tetrazole ring cleavage. It was demonstrated that these transformations can be used in the synthesis of anomalous nucleosides

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2006, 55 (11), 2071.pdf
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20.
Инвентарный номер: нет.
   
   I-85

   
    Isomerization of monohydroperfluoroalkenes [Electronic resource] / T. I. Filyakova, A. Ya. Zapevalov, M. I. Kodess, M. A. Kurykin, L. S. German // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1994. - Vol. 43, № 9. - P1526-1531
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Isomerization of monohydroperfluoro-1-alkenes HC(CF2)nCF=CF2 (n = 2 to 8) catalyzed by Lewis bases or acids (CsF, KHF2, and SbF5) under conditions of thermodynamic control affords equilibrium mixtures of all of the possible isomers resulting from migration of the double bond along the carbon chain. Under conditions of kinetic control, isomerization through the action of SbF5 gives -H-perfluoro-2-alkenes. The substantially higher proportion ofcis-isomers in the resulting monohydroperfluoroalkenes than in their perfluorinated analogs has been attributed to the effect of an intramolecular hydrogen bond

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\1994, 43 (9), 1526.pdf
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  БХЛ - Фонд художественной литературы

  ИИиА -Фонд исторической литературы в ЦНБ УрО РАН

  ИМЕТ -Отдел ЦНБ в Институте металлургии УрО РАН

  кх - Отдел фондов (книгохранениe)

  МБА - Межбиблиотечный абонемент

  мф - Методический фонд

  ок - Отдел научной каталогизации

  оку - Отдел комплектования и учета

  орф - Обменно-резервный фонд

  пф - Читальный зал деловой и патентной информации

  рк - Фонд редкой книги

  ч/з - Главный читальный зал

  эр - Зал электронных ресурсов

  

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