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Каталог книг и продолжающихся изданий
Сводный каталог иностранных периодических изданий, имеющихся в библиотеках УрО РАН
Сводный каталог отечественных периодических изданий, имеющихся в библиотеках УрО РАН
Каталог диссертаций и авторефератов диссертаций УрО РАН
Каталог препринтов УрО РАН (1975 г. - )
Имидж-каталог отечественных книг (до 2010 г.)
Имидж-каталог иностранных книг (до 2010 г.)
Алфавитно-предметный указатель (АПУ) ЦНБ УрО РАН
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Изобретения уральских ученых
Интеллектуальная собственность (статьи из периодики)
Нанотехнологии
Демидовские премии
Гибель династии Романовых
История Урала
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Книжная коллекция Шубиных
Труды Института высокотемпературной электрохимии УрО РАН
Труды Института истории и археологии УрО РАН
Труды сотрудников Института горного дела УрО РАН
Труды сотрудников Института органического синтеза УрО РАН
Труды сотрудников Института теплофизики УрО РАН
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Труды сотрудников ЦНБ УрО РАН
Публикации Черешнева В.А.
Публикации Чарушина В.Н.
Каталог библиотеки ИЭРиЖ УрО РАН
Электронная энциклопедия «Дискурсология»
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1.
Инвентарный номер: нет.
   
   S 89

   
    Structure of 5,6,7,8-tetrafluoro-4-hydroxycoumarins [Электронный ресурс] / K. V. Scherbakov, Ya. V. Burgart, M. I. Kodess, V. I. Saloutin // Chemistry of Heterocyclic Compounds. - 2012. - Vol.48, №9. - P1297-1306
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
5,6,7,8-TETRAFLUORO-4-HYDROXYCOUMARIN -- IMINE-ENAMINE TAUTOMERISM -- KETO-ENOL TAUTOMERISM
Аннотация: The structure of 5,6,7,8-tetrafluoro-4-hydroxycoumarin and its 3-substituted derivatives was studied by X-ray structural analysis and IR, 1H, 13C, and 15N NMR spectroscopy. It was established that the nature of the substituent at the position 3 of the coumarin ring has a significant effect on its stru

\\\\Expert2\\NBO\\Chemistry of Heterocyclic Compounds\\2012, v.48, N 9, p.1297-1306.pdf
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2.
Инвентарный номер: нет.
   
   R 30

   
    Reactions of perfluoro(2,3-epoxy-2-methylpentane) with o-phenylenediamine and ethylenediamine [Electronic resource] / T. I. Filyakova, A. Ya. Zapevalov, M. I. Kodess, P. A. Slepukhin, V. I. Saloutin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2013. - Vol.49, №3. - С. 350-355. - Библиогр.: с. 355 (16 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
O-PHENYLENEDIAMINE -- ETHYLENEDIAMINE -- C-N BOND
Аннотация: Perfluoro(2,3-epoxy-2-methylpentane) reacted with o-phenylenediamine and ethylenediamine via cleavage of the C-C bond to produce 2,2,3,3,3-pentafluoro-N-[2-(2,2,2-trifluoro-1-trifluoromethylethylamino)-phenyl]propanamide and 2,2,3,3,3-pentafluoro-N-[2-(2,2,2-trifluoro-1-trifluoromethylethylamino)ethyl]-propanamide, respectively. Presumably, these compounds are formed as a result of rearrangement of intermediate ketone generated by intramolecular haloform-type reaction. According to the NMR and X-ray diffraction data, 2,2,3,3,3-pentafluoro-N-[2-(2,2,2-trifluoro-1-trifluoromethylethylamino)phenyl]propanamide in crystal exists as Z conformer with respect to the amide C-N bond

\\\\expert2\\NBO\\Russian Journal of Organic Chemistry\\2013, 49, (3), 350-355.pdf
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3.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis of poly[N-(2,3-dihydroxypropyl)aminostyrene], a new sorbent for boron(III) ions / D. V. Nesterov, L. S. Molochnikov, M. I. Kodess, E. G. Matochkina, O. V. Koryakova, Yu. G. Yatluk, A. V. Pestov // Russian Journal of Applied Chemistry. - 2013. - Vol.86, №5. - С. 777-781. - Библиогр.: с. 781 (33 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
AMINOSTYRENE -- NITRATION -- GLYCIDOL
Аннотация: A procedure was developed for preparation of poly[N-(2,3-dihydroxypropyl)aminostyrene] via successive stages of nitration, reduction, and glycidol treatment of polystyrene, which gives the polymer with a maximal degree of functionalization. The composition and structure of the intermediates and end products of the polymer-analogous reactions were characterized by elemental analysis, IR spectroscopy, and solid-state 13C NMR spectroscopy. The sorption characteristics of poly[N-(2,3-dihydroxypropyl)aminostyrene] toward boroncontaining ions were assessed

\\\\expert2\\NBO\\Russian Journal of Applied Chemistry\\2013, v. 86, N 5, p.777.pdf
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4.
Инвентарный номер: нет.
   
   T 82

   
    Trans-Dichlorobis{(1R,4S)-1,7,7-trimethyl-3-[(S)-α-methylbenzylimino]bicyclo[2.2.1]heptan-2-one-N}Palladium(II): Synthesis and structural examination [Electronic resource] / O. A. Zalevskaya, O. A. Gur'eva, L. L. Frolova, I. N. Alekseev, P. A. Slepukhin, A. V. Kuchin // Russian Journal of Coordination Chemistry. - 2013. - Vol.39, №1. - P37-40
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
PALLADIUM(II) -- SYNTHESIS -- STRUCTURAL EXAMINATION
Аннотация: A reaction of (1R,4S)-1,7,7-trimethyl-3-[(S)-α-methylbenzylimino]bicyclo[2.2.1]heptan-2-one with lithium tetrachloropalladate gave a chiral palladium(II) complex with monodentate coordination of the organic ligand. The structure of the complex was confirmed by NMR spectra and X-ray diffraction data

\\\\Expert2\\NBO\\Russian Journal of Coordination Chemistry\\2013, v. 39, N. 1, p.37.pdf
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5.
Инвентарный номер: нет.
   

   
    σH-Adducts of 1-alkyl-1,4-diazinium salts as the sources of biradicals in the synthesis of tetraazaphenanthrenes / E. V. Verbitskiy, P. A. Slepukhin, M. A. Ezhikova, M. I. Kodess, Yu. N. Shvachko, D. V. Starichenko, G. L. Rusinov, V. N. Charushin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2011. - Vol.60, №5. - С. 975-980
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
PH-ADDUCTS -- BIRADICALS -- TETRAAZAPHENANTHRENES
Аннотация: O- and C-Adducts of 5-(het)aryl-2,3-dicyano-1-ethylpyrazinium salts are latent sources of biradicals capable of forming tetraazaphenanthrene derivatives via dimerization. The mechanisms of the reactions were examined using ESR spectroscopy. The stereochemistry of the resulting heterocyclic systems was studied by NMR spectroscopy. The crystallographic data on their three-dimensional structures were obtained

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2011, 60 (5), 975-980.pdf
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6.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis of regioisomeric N- and O-alkylated 3-polyfluoroalkyl-1,2-dihydroquinoxalin-2-o / A. E. Ivanova, O. G. Khudina, Ya. V. Burgart, V. I. Saloutin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2011. - Vol.60, №5. - С. 937-941
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SYNTHESIS -- DIHYDROQUINOXALIN -- POLYFLUOROALKYL
Аннотация: 3-Polyfluoroalkyl-1,2-dihydroquinoxalin-2-ones react with 4-bromobutyl acetate to furnish 1-(4-acetoxybutyl)quinoxalin-2-ones and 2-(4-acetoxybutoxy)quinoxalines in the ratio 2: 1. Deacylation of these compounds under acidic conditions gives the corresponding 1-(4-hydroxybutyl)- and 2-(4-hydroxybutoxy)-substituted quinoxalines. The structures of compounds synthesized were established by X-ray crystallography, IR spectroscopy, 1H and 19F NMR spectroscopy, GLC-MS

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7.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis of novel fluorine- and iodine-containing [1,2,4]triazolo[3,4-b][1,3]thiazines based 3-(alkenylthio)-5-(trifluoromethyl)-4H-1,2,4-triazole-3-thiols [Electronic resource] / E. S. Ilinykh, D. G. Kim, M. I. Kodess, E. G. Matochkina, P. A. Slepukhin // Journal of Fluorine Chemistry. - 2013. - Vol.149. - P24-29
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SYNTHESIS -- FLUORINE-CONTAINING -- IODIDES
Аннотация: In this paper we report the synthesis of novel S-alkenyl derivatives of 5-(trifluoromethyl)-4H-1,2,4-triazole-3-thiol via alkenation reaction with different alkenyl halides. Reaction between the resulting S-alkenation products and iodine proceeds regiospecifically to give new fused fluorine- and iodine-containing [1,2,4]triazolo[3,4-b][1,3]thiazine heterocyclic systems. The structure of synthesized compounds was confirmed by mass spectra, IR, 1H, 13C and 19F NMR spectroscopy including 2D 1H–13C HSQC, 1H–1H COSY, 1H–13C HMBC correlations, elemental analysis and single-crystal X-ray diffraction study. --------------------------------------------------------------------------------

\\\\Expert2\\NBO\\Journal of Fluorine Chemistry\\2013, v. 149, p.24.pdf
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8.
Инвентарный номер: нет.
   
   I-55

   
    Imidazole-containing chitosan derivative: a new synthetic approach and sorption properties [Electronic resource] / A. V. Pestov, S. YU. Bratskaya, Yu. A. Azarova, Yu. G. Yatluk // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2012. - Vol.61, №10. - С. 1959-1964. - Bibliogr. : p. 1963-1964 (33 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CHITOSAN -- SORBENT -- GOLD(III)
Аннотация: A novel method for the synthesis of a hetaryl containing chelate amino polymer, namely, N (4(5) imidazolylmethyl)chitosan (IMC), with a degree of substitution up to 0.3 was pro posed. The "synthesis in gel" approach involves direct substitution of the hydroxyl group in 4(5) imidazolylmethanol. The structures of these polymers were confirmed by 1H NMR data. For sorption studies, IMC samples were crosslinked with epichlorohydrin and diglycidyl ethers of ethylene glycol and diethylene glycol. The degrees of swelling and sorption properties of the polymers largely depend on the crosslinking agent and the degree of crosslinking. The sorption capacities of IMC for AuIII, PtIV, and PdII ions are higher than those of the nonmodified polymer. The extraction of noble metal ions from chloride solutions becomes more selective with increasing degree of crosslinking. The sorption capacity of IMC for CoII and NiII ions is higher than those of chitosan and its known N heterocyclic derivatives

\\\\expert2\\NBO\\Russian Chemical Bulletin\\2012, 61 (10), 1959-1964.pdf
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9.
Инвентарный номер: нет.
   
   R 35

   
    Regioselective reaction of ortho-piperidinobenzaldehydes with pyrazolone [Electronic resource] / A. Yu. Platonova, E. V. Deeva, O. A. Zimovets, D. V. Shatunova, O. S. Eltsov, P. A. Slepukhin, T. V. Gluchareva, Yu. Yu. Morzherin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2011. - Vol.60, №5. - С. 961-964. - Bibliogr. : p. 964 (20 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
TERT-AMINO EFFECT -- PYRAZOLONE -- DIASTEREOMERS
Аннотация: Cyclization of 2 (4 R piperidino)benzaldehydes with 5 methyl 2 phenyl 2,4 dihydro 3H pyrazol 3 one proceeding via tert amino effect mechanism is stereoselective. Relative configu ration of (3R*,4aS*,5R*) 2,3,4,4a,5,6 hexahydro 1H benzo[c]quinolizine was established on the base of NMR spectroscopy data and X ray analysis

\\\\expert2\\NBO\\Russian Chemical Bulletin\\2011, 60 (5), 961-964.pdf
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10.
Инвентарный номер: нет.
   
   S 90

   
    Study of oligomeric compounds of Urea-fotmaldehyde concentrate by ESI MS, IR and NMR spectroscopy / S. Y. Men'shikov, I. N. Ganebnuikh, M. S. Valova, L. S. Molochnikov // European Polymer Congress, Pisa, June 16-21 2013 : book of abstracts . - Pisa, Italy, 2013. - P2-107
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SPECTROSCOPY -- OLIGOMERIZATION PRODUCTS -- NMR SPECTRA

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11.
Инвентарный номер: нет.
   
   R 30

   
    Reactions of 1,1,1trihalo-3-nitrobut-2-enes with enamines derived [Electronic resource] / V. Yu. Korotaev, A. Yu. Barkov, P. A. Slepukhin, V. Ya. Sosnovskikh // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2012. - Vol.61, №9. - С. 1750-1760. - Bibliogr. : p. 1760 (30 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
1,1,1TRIHALO-3NITROBUT-2ENES -- ENAMINES -- X-RAY DIFFRACTION
Аннотация: 1,2 Oxazine Noxides derived from (E)1,1,1trifluoro3nitrobut2ene and cyclohexanone enamines underwent spontaneous rearrangement with ring contraction to give 1pyrroline N oxides. Reactions of (E) 1,1,1 trifluoro(trichloro) 3 nitrobut 2 enes with N cyclopent enylmorpholine resulted in a series of novel CX3 containing nitroalkyl enamines and g nitro ketones; the stereochemistry of the synthesized compounds were studied by NMR spectroscopy and X ray diffraction

\\\\expert2\\NBO\\Russian Chemical Bulletin\\2012, 61 (9), 1750-1760.pdf
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12.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis in a gel and sorption properties of N-2-sulfoethyl chitosan / A. V. Pestov, Yu. S. Petrova, A. V. Bukharova, L. K. Neudachina, O. V. Koryakova, E. G. Matochkina, M. I. Kodess, Yu. G. Yatluk // Russian Journal of Applied Chemistry. - 2013. - Vol.86, №2. - С. 269-272. - Библиогр.: с. 272 (24 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CHELATES -- AMINO-CONTAINING POLYMER -- N-2-SULFOETHYL CHITOSAN
Аннотация: A new procedure was developed for preparation of chelate amino-containing polymer N-2-sulfoethyl chitosan by synthesis in a gel through the reaction between chitosan and sodium 2-bromoethanesulfonate, yielding a polymer with the degree of substitution of up to 0.5. The structure of the resulting polymers was confirmed by 1H NMR spectroscopy. The sorption characteristics with respect to transition and alkaline-earth metal ions were determined for the cross-linked polymers

\\\\expert2\\NBO\\Russian Journal of Applied Chemistry\\2013, v. 86, N 2, p.269.pdf
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13.
Инвентарный номер: нет.
   
   L 87

   
    Long-range 1H-15N J couplings providing a method for direct studies of the structure and azide-tetrazole equilibrium in a series of azido-1,2,4-triazines and azidopyrimidines [Electronic resource] / T. S. Shestakova, Z. O. Shenkarev, S. L. Deev , O. N. Chupakhin, L. A. Khamidullina, V. L. Rusinov, A. S. Arseniev // Journal of Organic Chemistry. - 2013. - Vol.78, №14. - P6975-6982. - Библиогр.: с. 6981-6982 (43 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
AMPLITUDE-MODULATED -- COUPLING CONSTANTS -- NITROUS ACID
Аннотация: The selectively 15N labeled azido-1,2,4-triazine 2*A and azidopyrimidine 4*A were synthesized by treating hydrazinoazines with 15N-labeled nitrous acid. The synthesized compounds were studied by 1H, 13C, and 15N NMR spectroscopy in DMSO, TFA, and DMSO/TFA solutions, where the azide-tetrazole equilibrium could lead to the formation of two tetrazoles (T, T′) and one azide (A) isomer for each compound. The incorporation of the 15N label led to the appearance of long-range 1H-15N coupling constants (JHN), which can be measured easily by using amplitude-modulated 1D 1H spin-echo experiments with selective inversion of the 15N nuclei. The observed JHN patterns enable the unambiguous determination of the mode of fusion between the azole and azine rings in the two groups of tetrazole isomers (2*T′, 4*T′ and 2*T, 4*T), even for minor isoforms with a low concentration in solution. However, the azide isomers (2*A and 4*A) are characterized by the absence of detectable J HN coupling. The analysis of the JHN couplings in 15N-labeled compounds provides a simple and efficient method for direct NMR studies of the azide-tetrazole equilibrium in solution

\\\\expert2\\NBO\\Journal of Organic Chemistry\\2013, v.78, p.6975.pdf
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14.
Инвентарный номер: нет.
   
   R 30

   
    Reaction of (E)-1,1,1-trichloro-3-nitrobut-2-ene with amines: diastereoselective synthesis of N-substituted α-trichloromethyl-β-nitroamines [Electronic resource] / A. Yu. Barkov, V. Yu. Korotaev, P. A. Slepukhin, M. I. Kodess, V. Ya. Sosnovskikh // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2012. - Vol.61, №8. - С. 1564-1569. - Bibliogr. : p. 1569 (22 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
NITROALKENES -- AMINES -- MICHAEL REACTION
Аннотация: The addition of primary and secondary amines to (E) 1,1,1 trichloro 3 nitrobut 2 ene proceeded diastereoselectively and led to a number of new N substituted  trichloromethyl  nitroamines, whose stereochemistry was confirmed by X ray crystallography and NMR spec troscopy

\\\\expert2\\NBO\\Russian Chemical Bulletin\\2012, 61 (8), 1564-1569.pdf
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15.
Инвентарный номер: нет.
   
   U 62

   
    Unusual heterocyclization of chalcone podands with 3-amino-1,2,4-triazole / I. G. Ovchinnikova, M. S. Valova, E. G. Matochkina, M. I. Kodess, A. A. Tumashov, P. A. Slepukhin, O. V. Fedorova, G. L. Rusinov, V. N. Charushin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2011. - Vol.60, №5. - С. 965-974
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
TEMPLATE SYNTHESIS -- CHALCONE PODAND -- CROWN ETHERS
Аннотация: A new type of intramolecular cyclization of 1,5-bis[2-(E-3-oxo-3-phenylprop-1-enyl)-phenoxy]-3-oxapentane with 3-aminotriazole promoted by potassium ions was discovered. A cascade mechanism for the formation of crownophane with 4,7-dihydro[1,2,4]triazolo[1,5-a]-pyrimidine fragment was suggested. Effects of oligooxyethylene fragment of the chalcone podand and acid-base catalysis on the selectivity of the cyclocondensation processes and degree of oxidation of triazolopyrimidine fragments were studied. The product structures were confirmed by IR, 1H and 13C NMR spectroscopy and X-ray diffraction study

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2011, 60 (5), 965-974.pdf
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16.
Инвентарный номер: нет.
   
   O-57

   
    One-pot synthesis of trifluoromethyl- and nitroso-substituted pyrazolines and pyrazoles and their tuberculostatic activity [Electronic resource] / O. G. Khudina, Ya. V. Burgart, V. I. Saloutin, M. A. Kravchenko // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2010. - Vol. 59, № 10. - P1967-1973. - Bibliogr. : p. 1973 (14 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: 3-Trifluoromethyl-substituted 4-nitrosopyrazolines and 4-nitrosopyrazoles were prepared by a one-pot synthesis from trifluoromethyl-containing 1,3-diketones, sodium nitrite in acetic acid, and hydrazines (hydrazine hydrate, methylhydrazine). 3-Trifluoromethylpyrazolines can be converted to pyrazoles on heating. The use of phenylhydrazine in these reactions led to the formation of regioisomeric 4-hydroxyimino-5-(trifluoromethyl)pyrazoline. The structure of heterocycles synthesized was established using X-ray diffraction study, 1H and 19F NMR spectroscopy. The obtained products exhibited considerable tuberculostatic activity

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2010, 59 (10), 1967-1973.pdf
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17.
Инвентарный номер: нет.
   
   U 52

   
    Unexpected dimerization of 5,7-dimethyl-2-trifluoromethyl-8-azachromone induced by hydrogen sulfide [Electronic resource] / M. A. Barabanov, V. Ya. Sosnovskikh, V. S. Moshkin, M. I. Kodess // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2010. - Vol. 59, № 11. - P2094-2097. - Bibliogr. : p. 2097 (18 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Depending on the reaction conditions, the reaction of 5,7-dimethyl-2-trifluoromethyl-8-azachromone with hydrogen sulfide afforded cyclic and linear dimers with the S-S bond. The regio- and stereochemistry of the reaction products were determined by 1H and 13C NMR spectroscopy

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2010, 59 (11), 2094-2097.pdf
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18.
Инвентарный номер: нет.
   
   C 74

   
    Composition, structure, and properties of pharmacologically active silicon dimethylglycerolates [Electronic resource] / T. G. Khonina, E. Yu. Larchenko, E. V. Shadrina, I. N. Ganebnuikh, A. A. Boyko, E. G. Matochkina, M. I. Kodess, O. N. Chupakhin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2010. - Vol. 59, № 12. - P2230-2235. - Bibliogr. : p. 2235 (13 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: 1H and 29Si NMR spectroscopy showed that the product of the reaction of dimethyldiethoxysilane with glycerol in the molar ratio 1: 2 is an equilibrium mixture of dimethyldiglyceroxysilane and low-molecular-weight condensation products. The change of viscosity of silicon dimethylglycerolates, synthesized using different excesses of glycerol, versus time was studied by viscosimetry. Composition of products of hydrolysis and condensation of silicon dimethylglycerolates is determined by their concentration in the starting aqueous solutions

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2010, 59 (12), 2230-2235.pdf
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19.
Инвентарный номер: нет.
   
   A 90

   
    Atropoisomerism of 13-N,N-dimethylamide-15,17-dimethyl ester of chlorin e6 from the data of X-ray, 1H NMR, and HPLC [Electronic resource] / D. V. Belykh, E. V. Buravlev, P. A. Slepukhin, A. V. Kuchin // Russian Journal of General Chemistry. - 2010. - Vol. 80, № 11. - P2382-2386. - Bibliogr. : p. 2386 (9 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Atropoisomerism of tertiary 13-amides of chlorin e 6 was studied by the methods of X-ray analysis, 1H NMR spectroscopy, and high performance liquid chromatography on the example of 13-N,N-dimethylamide-15,17-dimethyl ester of chlorin e 6. The spatial structure of the major and minor atropoisomers was established. The possibility of reversible interconversion of the atropoisomers of the studied compound in solution was shown

\\\\Expert2\\nbo\\Russian Journal of General Chemistry\\2010, V. 80, N 11, p.2382-2386.pdf
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20.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis, characterization and ethylene oligomerization studies of nickel(II) based new formazane derivatives [Text] / A. V. Zaidman, I. G. Pervova, A. I. Vilms, G. P. Belov, R. R. Kayumov, P. A. Slepukhin, I. N. Lipunov // Inorganica Chimica Acta. - 2011. - Vol. 367, № 1. - P29-34
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: A series of nickel(II) complexes based novel mono- and bis-formazan ligands has been synthesized and characterized with IR, UV, NMR spectroscopies, CHN analysis, mass spectrometry, and single crystal X-ray diffraction analysis. The prepared complexes have been tested for catalytic activity in ethylene oligomerization

\\\\Expert2\\nbo\\Inorganica Chimica Acta\\2011, v. 367, p.29.pdf
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