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Каталог книг и продолжающихся изданий
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Каталог диссертаций и авторефератов диссертаций УрО РАН
Каталог препринтов УрО РАН (1975 г. - )
Имидж-каталог отечественных книг (до 2010 г.)
Имидж-каталог иностранных книг (до 2010 г.)
Алфавитно-предметный указатель (АПУ) ЦНБ УрО РАН
Публикации об УрО РАН
Изобретения уральских ученых
Интеллектуальная собственность (статьи из периодики)
Нанотехнологии
Демидовские премии
Гибель династии Романовых
История Урала
Личная библиотека С. В. Вонсовского
Книжная коллекция Шубиных
Труды Института высокотемпературной электрохимии УрО РАН
Труды Института истории и археологии УрО РАН
Труды сотрудников Института горного дела УрО РАН
Труды сотрудников Института органического синтеза УрО РАН
Труды сотрудников Института теплофизики УрО РАН
Труды сотрудников Института химии твердого тела УрО РАН
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Труды сотрудников ЦНБ УрО РАН
Публикации Черешнева В.А.
Публикации Чарушина В.Н.
Каталог библиотеки ИЭРиЖ УрО РАН
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1.
Инвентарный номер: нет.
   
   Ч-54

   
    4,5-Difluoro-1,2-dehydrobenzene: generation and cycloaddition reactions [Electronic resource] / V. N. Charushin, S. K. Kotovskaya, S. A. Romanova, O. N. Chupakhin, Yu. V. Tomilov, O. M. Nefedov // Mendeleev Communications. - 2005. - Vol. 15, № 2. - P45-46
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CYCLOADDITION REACTIONS
Аннотация: The oxidation of 1-amino-5,6-difluorobenzotriazole with Pb(OAc)4 in dry CH2Cl2 afforded 4,5-difluoro-1,2-dehydrobenzene, a new active intermediate, which can be used in situ for the synthesis of fluorinated carbo- and heterocyclic compounds via cycloaddition reactions.

\\\\Expert2\\nbo\\Mendeleev Communications\\2005, v.15, p.45.pdf
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2.
Инвентарный номер: нет.
   
   A 10

   
    A versatile strategy for the synthesis of functionalized 2,2 '-bi- and 2,2 ': 6 ',2 '-terpyridines via their 1,2,4-triazine analogues [Text] / V. N. Kozhevnikov, D. N. Kozhevnikov, T. V. Nikitina, V. L. Rusinov, O. N. Chupakhin, M. Zabel, B. Konig // Journal of Organic Chemistry. - 2003. - Vol. 68, № 7. - P2882-2888
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ALDEHYDES -- OXIDATION -- SUBSTITUTION REACTIONS
Аннотация: A general synthetic route for the synthesis of functionalized bi- and terpyridines is reported. Functionalized 1,2,4-triazene 4-oxides 7 and 8 - obtained from the reaction of hydrazones 1 with pyridine aldehydes and followed by oxidation - are functionalized by introduction of a cyano group via nucleophilic aromatic substitution. The thus-obtained 5-cyano-1,2,4-triazines 9 and 10 undergo facile inverse-electron-demand Diels-Alder reactions with enamines and alkenes to yield functionalized bi- and terpyridines, respectively. The substituent at position 6 of the 1,2,4-triazene 4-oxides must be aromatic or heteroaromatic in order to allow their facile synthesis, but other substituents and reagents may vary. Each step of the synthetic route allows diversification, which makes the approach particularly useful for the facile synthesis of a large variety of functionalized bi- and terpyridines.

\\\\Expert2\\nbo\\Journal of Organic Chemistry\\2003, v.68, N 7, p.2882. Chupakhin.pdf
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3.
Инвентарный номер: нет.
   
   A 53

   
    Analysis of the Gas Phase Oxidation Methanol at Presence of the Catalyst on Base of FeMoO4 / S. Y. Men'shikov, A. A. Markov, M. S. Valova, V. A. Vazhenin, A. A. Subbotina, J. V. Trubnikova // Уральский научный форум "Современные проблемы органической химии". XVII Молодежная школа-конф. по органической химии, Екатернинбург, 8-12 июня 2014 г. : сб. тез. - Екатеринбург, 2014. - С. 174
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
METHANOL -- FeMoO4 -- MOLYBDENUM-OXIDE

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4.
Инвентарный номер: нет.
   
   A 89

   
    Asymmetric oxidation of hetaryl neomenthyl sulfides / M. Ya. Demakova, D. V. Sudarikov, S. A. Rubtsova, P. A. Slepukhin, A. V. Kutchin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2012. - Vol.48, №1. - С. 113-118
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ASYMMETRIC OXIDATION -- SULFIDES
Аннотация: Previously unknown diastereoisomeric sulfoxides were synthesized by asymmetric oxidation of 2-neomenthylsulfanyl-substituted 1H-imidazole, 1-methyl-1H-imidazole, and 1H-benzimidazole

\\\\Expert2\\nbo\\Russian Journal of Organic Chemistry\\2012, 48 (1), 113-118.pdf
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5.
Инвентарный номер: нет.
   
   A 89

   
    Asymmetrical oxidation of menthone dithiolane [Electronic resource] / A. V. Timshina, S. A. Rubtsova, M. I. Kodess, E. G. Matochkina, P. A. Slepukhin, A. V. Kuchin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2008. - Vol. 44, № 7. - P1043-1048
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Asymmetrical oxidation was performed of menthone dithiolane obtained in 95–98% yield by condensation of menthone with 1,2-ethanedithiol in the presence of boron trifluoride etherate. 6-Isopropyl-9-methyl-1,4-dithiaspiro[4,5]decane-1,4-dioxide (yield 5–55%) and 6-isopropyl-9-methyl-1,4-dithiaspiro[4,5]-decane-1,1,4-trioxide (yield 65–70%) were synthesized. Chemical structures of compounds obtained were proved by XRD analysis, NMR and IR spectroscopy

\\\\Expert2\\nbo\\Russian Journal of Organic Chemistry\\2008, 44 (7), 1043.pdf
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6.
Инвентарный номер: нет.
   
   C 31

   
    Catalytic activity and electrochemical properties of chitosan-containing materials [Text] : реферат / E. G. Kovaleva, A. V. Pestov, A. Mechaev, L. S. Molochnikov, V. Chetina // 6-th Kenya Chemical Society " East and Southern Africa Environmental chemistry", 8-th Theoretical Chemistry in Africa International conference, Kenya, Mombasa, 5-9 Oct. 2009. : вook of abstracts . - Mombasa, Kenya, 2009. - P. 22.
УДК
54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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7.
Инвентарный номер: нет.
   

    Chupakhin, O. N.
    Application of electrochemical oxidative methods in the C(SP2)–H functionalization of heterocyclic compounds / O. N. Chupakhin, A. V. Shchepochkin, V. N. Charushin // Advances in heterocyclic chemistry. - 2020. - Т. 131. - P1-47
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
C-H FUNCTIONALIZATION -- ELECTROCHEMICAL OXIDATION -- GREEN CHEMISTRY -- OCDC -- SN H REACTIONS
Аннотация: New atom-economic and environmentally friendly processes should replace the traditional ways of building C–C, C–N, C–O, C–P, C–S bonds, which are usually based on the replacement of a halogen atom, and, therefore, required the preliminary modification of substrates, and the use of aggressive reagents, harsh conditions or expensive catalysts. In recent years, the direct metal-free functionalization of the C(sp2)–H bond, which provides the most efficient and low-waste pathway for molecular transformation, has attracted increasing attention. However, these transformations usually require stoichiometric amounts of chemical oxidizing agents. The modern world and its sustainable development trends are forcing the chemical industry to improve in an environmentally friendly direction and meet the requirements of “green chemistry.” In this regard, the use of electrochemical methods is extremely important. Electrochemical anodic oxidation is an ideal option for the replacement of chemical oxidizers in C–H functionalization reactions. The data on the main electrochemical methods and approaches used for the direct functionalization of the C(sp2)–H bond in heterocyclic compounds are classified and summarized in this paper.

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8.
Инвентарный номер: нет.
   
   C 76

   
    Convenient synthesis of building-blocks for pyridine/piperidine-decorated crown ethers [Electronic resource] / M. B. Nawrozkij, E. B. Gorbunov, V. L. Rusinov, V. N. Charushin // Macroheterocycles . - 2014. - Vol.7, №1. - С. 18-22. - Bibliogr. : p. 22 (19 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
2-VYNYLPYRIDINE -- EPOXIDATION -- HYDROXYLATION
Аннотация: A convenient way to 1-(pyridin-2-yl)ethan-1,2-diol, 2-(oxiran-2-yl)pyridine and two diastereomeric forms of 1-(piperidin- 2-yl)ethan-1,2-diol, valuable building-blocks for the synthesis of functionalized crown ethers, has been developed. It is based on the Wagner oxidation or NBS-mediated epoxydation of 2-vinylpyridine, and the Schwenk-Papa reduction of 1-(pyridin-2-yl)ethan-1,2-diol, accompanied by fractional crystallization of a diastereo-meric mixture of the target product

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9.
Инвентарный номер: нет.
   
   D 46

   
    Design and Synthesis of N-Sulfonylamidines of Modafinic Acid [Electronic resource] / T. Beryozkina, V. A. Bakulev, L. Dianova, P. A. Slepukhin // Synthesis-Stuttgart. - 2016. - Vol. 48, № 7. - С. 1046-1054
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
MODAFINIL -- N-SULFONYL AMIDINES -- DAT INHIBITORS
Аннотация: A design and a convenient approach for the synthesis of novel N-sulfonyl-2-diphenylmethylsulfinylacetamidines have been demonstrated by starting from benzhydrylsulfanylacetic (BSA) acid. This approach involves a sequential amidation with amines, thionation with Lawesson's reagent, iminosulfonylation with sulfonyl azides, and oxidation of sulfide fragment with hydrogen peroxide. The key step of this transformation (reaction of thioamides with sulfonyl azides) was carried out either in ethanol or in the absence of any solvent. The synthesized compounds were tested in cells for inhibition of dopamine transporter. Among the synthesized compounds, two products were found to be in a similar range of activity as the well-known dopamine transporter inhibitor, modafinil.

\\\\expert2\\NBO\\Synthesis-Stuttgart\\2016. 48(7). 1046-1054.pdf
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10.
Инвентарный номер: нет.
   
   D 62

   
    Direct modification of benzoannelated crown ethers with 1,2,4-triazin-5(2H)-one moieties [Text] / G. L. Rusinov, D. G. Beresnev, N. A. Itsikson, O. N. Chupakhin // Heterocycles. - 2001. - Т. 55, № 12. - P2349-2359
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: A convenient method for one-step coupling of benzoannelated crown ethers with 1,2,4-triazinones based on the reaction of nucleophilic addition to unsubstituted carbon atom of the triazine ring has been worked out. It has been shown that the reaction of 3-substituted 1,2,4-triazin-5(2H)-ones (1) with benzocrown ethers (benzo-12-crown-4, benzo-15-crown-5, benzo-18-crown-6) in the presence of acetic or trifluoroacetic anhydride is accompanied by acylation of triazine ring and results in formation of 3-(1-acyl-5-oxo-1,4,5,6-tetrahydro-1,2,4-triazin-6-yl)benzocrown ethers (7-12). The latters were converted to 3-(5-oxo-2,5-dihydro-1,2,4-triazin-6-yl)benzocrown ethers (18-20) using two alternative routes: the elimination of acetic or trifluoroacetaldehyde or the deacylation followed by the oxidation of the 1,4,5,6-tetrahydro derivatives (13-15).

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11.
Инвентарный номер: нет.
   
   E 43

   
    Electrochemical sensor based on metal-containing receptors for urea measurements [Text] : доклад, тезисы доклада / A. Kozitsina [и др.] // International Congress on Analytical Sciences "ICAS - 2006",M., June 25-30 2006 : book of abstracts. - М., 2006. - Vol. 1. - P291 : табл. - Bibliogr. : p. 291 (1 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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12.
Инвентарный номер: нет.
   
   E 43

   
    Electronic structure of CrxTi1-xX2, X = S, Se solid solutions / A. I. Merentsov, Yu. M. Yarmoshenko, A. N. Skorikov, A. N. Titov, A. Buling, M. Rakers, M. Neumann, E. G. Galieva, P. A. Slepukhin // Journal of Electron Spectroscopy and Related Phenomena. - 2010. - Vol. 182, № 1-2. - С. 70-75. - Bibliogr. : p. 74-75 (13 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ELECTRONIC STRUCTURE -- DOS -- SPIN POLARIZATION
Аннотация: We synthesize CrxTi1-xSe2 (x = 0–0.83) and CrxTi1-xS2 (x = 0.3–0.4) systems and study the structure of these materials on mono- and polycrystalline samples. It appeared that an increase in chromium content leads to inversion of titanium diselenide intercalated with chromium to chromium diselenide intercalated with titanium. The XPS of core levels and valence bands of 1T-CrxTi1-xSe2 and CrxTi1-xS2 was also investigated and it was shown that in in-layer and inter-layer positions the atoms of chromium and titanium are characterized by a slightly differing oxidation state. Chromium LDOS model calculations were carried out and the results being in agreement with the experimental data show that the Cr 3d density of electronic states of chromium in Ti-positions in the host lattice displays half-metallic properties, while the Cr 3d density of electronic states of intercalated chromium is far from being half-metallic????

\\\\Expert2\\nbo\\Journal of Electron Spectroscopy and Related Phenomena\\2010, v.182, p.70.pdf
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13.
Инвентарный номер: нет.
   

   
    Expedient synthesis of 1,2,4-triazinyl substituted benzo[c]coumarins via double oxidation strategy / R. F. Fatykhov, I. A. Khalymbadzha, A. D. Sharapov [et al.] // Chimica Techno Acta. - 2023. - Vol. 10, № 2. - P202310205
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
COUMARIN -- 1,2,4-TRIAZINE -- NUCLEOPHILIC SUBSTITUTION OF HYDROGEN
Аннотация: Herein, we report a convenient one-pot synthesis of 1,2,4-triazinyl derivatives of benzocoumarins. The proposed approach consists of the nucleophilic addition of tetrahydrobenzo annulated dimethoxycoumarin to 1,2,4-triazines followed by double oxidation of both dihydrotriazine and tetrahydrobenzo groups with 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ). The nucleophilic addition of the dimethoxycoumarin to 1,2,4-triazines was carried out in the presence of three-fold excess of methanesulfonic acid in DCM at room temperature. It takes place between positions 8 and 5 of coumarin and 1,2,4-triazine, respectively. The double oxidation step was carried out with 3.6 equivalent of DDQ. Selective oxidation of dihydrotriazine moiety, without affecting the tetrahydrobenzo fragment, was achieved using 1.2 equivalent of tetrachlorobenzoquinone (TCQ). The differences in the oxidation with TCQ and DDQ appear to be related to the higher oxidative potential of DDQ in contrast to TCQ. The advantages of the method are the elimination of the use of transition metals, the availability of starting materials, and the simplicity of the procedure. The proposed approach provides a two-step one-pot protocol for the synthesis of triazinyl benzocoumarins, precursors for the preparation of push-pull pyridinyl chromophore.

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14.
Инвентарный номер: нет.
   
   F 76

   
    Formation of a cluster h2v10o 28 4– under the action oF Bronsted acids and its catalytic activity in oxidation of alkylbenzenes / M. I. Ul'yanova, M. G. Pervova, P. A. Slepukhin, A. V. Pestov, T. V. Aksenova // Russian Journal of Organic Chemistry. - 2018. - Vol. 54, № 5. - P687-690
ББК Г2
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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15.
Инвентарный номер: нет.
   
   K 96

    Kuznetsov, V. A.
    Synthesis of epsilon-caprolactone with stable hydrogen peroxide adducts / V. A. Kuznetsov, M. G. Pervova, Yu. G. Yatluk // Russian Journal of Applied Chemistry. - 2013. - Vol.86, №2. - С. 176-181. - Библиогр.: с. 181 (16 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CYCLOHEXANONE -- E-CAPROLACTONE -- HEXAFLUOROISOPROPANOL
Аннотация: Oxidation of cyclohexanone to ɛ-caprolactone with stable industrially manufactured hydrogen peroxide derivatives: adduct with urea (urea hydrogen peroxide), sodium perborate, sodium percarbonate (Persol), magnesium monoperphthalate (Dismozon) was studied. Oxidation with urea hydrogen peroxide is the most efficient in hexafluoroisopropanol in the case of preliminary removal of urea in the form of an oxalate. Oxidation with sodium perborate and percarbonate provides high yields in trifluoroacetic acid. The lowest cost process consists in interaction with sodium monoperphthalate (Persol and phthalic anhydride) in an aqueous medium

\\\\expert2\\NBO\\Russian Journal of Applied Chemistry\\2013, v. 86, N 2, p.176.pdf
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16.
Инвентарный номер: нет.
   
   L 79

   
    Liquid-phase oxidation of anthracene by hydrogen-peroxide in the presence of heterogenized vanadyl acetylacetonate [Electronic resource] / S. Y. Men'shikov, A. V. Vurasko, L. A. Petrov, L. S. Molochnikov, A. A. Novoselova, Z. E. Skryabina, V. I. Saloutin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1992. - Vol. 41, N 4. - P619-622
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: The synthesis of hetrogenized vanadyl acetylacetoonate was accomplished by alkylation of a chloromethylated styrene-divinylbenzene copolymer via activation by Co (II) complexes. The effect of heterogenization of the structure of the complexes and their catelytic properties in the peroxide oxidation of anthracene was investigated by kinetic studies and ERP spectroscopy

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\1992, 41 (4), 619.pdf
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17.
Инвентарный номер: нет.
   
   L 79

   
    Liquid-phase oxidation of anthracene by hydrogen-peroxide in the presence of vanadium-oxide bronzes CuXV2O5 [Text] / S. Y. Men'shikov, A. V. Vurasko, L. A. Petrov, V. L. Volkov, A. A. Novoselova // Pet-Chem Equipment Corp. - 1992. - Vol. 32, N 2. - P128-130
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Vanadium oxide bronzes of the general formula CuXV2O5, where 0x1, catalyse the liquid-phase oxidation of anthracene H2O2. The anthracene conversion and the selectivity with respect to anthraquinone are maximum withing the region of beta- and xi-phases respectively close to the compositions CuO. 6V2O5 and CuO.95V2O5.

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18.
Инвентарный номер: нет.
   
   L 79

   
    Liquid-phase oxidation of trimethylhydroquinone catalyzed by copper(II) chloride in the presence of cellulose inorganic composites [Text] : доклад, тезисы доклада / A. B. Shishmakov, Yu. V. Mikushina, M. S. Valova, O. V. Koryakova, L. A. Petrov // III International Conference "Catalysis: Fundamentals and Application", dedicated to the 100th anniversary of Academician G. K. Boreskov, Novosibirsk, July 4-8 2007 : abstr. . - Novosibirsk, 2007. - P97-98
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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19.
Инвентарный номер: нет.
   
   M 39

    Matern, A. I.
    Progress in the studies of oxidation of dihydropyridines and their analogues [Electronic resource] / A. I. Matern, V. N. Charushin, O. N. Chupakhin // Russian Chemical Reviews. - 2007. - Vol. 76, № 1. - P23-40
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Published data on oxidation of dihydropyridines and on the mechanisms and the role of hydride shifts in bioorganic chemistry, enantioselective synthesis and supramolecular chemistry are generalised.

\\\\Expert2\\nbo\\Russian Chemical Reviews\\2007, V.76, N1, p.23.pdf
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20.
Инвентарный номер: нет.
   
   N 91

   
    Nucleophilic dimerization of indoline under oxidative conditions [Electronic resource] / I. S. Kovalev, D. S. Kopchuk, G. V. Zyryanov, V. L. Rusinov, O. N. Chupakhin // Mendeleev Communications. - 2014. - Vol. 24, № 1. - С. 40-41
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
INDOLINE -- HYDROGEN PEROXIDE -- SODIUM TUNGSTATE AFFORDS
Аннотация: Oxidation of indoline with 30% hydrogen peroxide in methanol in the presence of sodium tungstate affords the dimeric 3-oxo-1’H,3H- 2,3’-biindole-1-oxide

\\\\expert2\\nbo\\Mendeleev Communications\\2014, v.24, p. 40-41.pdf
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  эр - Зал электронных ресурсов

  

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