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автору	заглавию	году издания	типу документа

Поисковый запрос: (<.>K=SILICON<.>)

Общее количество найденных документов : 28
Показаны документы с 1 по 20

1-20 21-28

Инвентарный номер: нет.

   N 52


    New hybrid chitosan–silicone-containing glycerohydrogels [Electronic resource] / E. Yu. Larchenko, E. V. Shadrina, T. G. Khonina, O. N. Chupakhin // Mendeleev Communications. - 2014. - Vol.24. - С. 201-202

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CHITOSAN -- GLYCEROHYDROGELS -- SILICON GLYCEROLATES
Аннотация: New biologically active hybrid chitosan–silicone-containing glycerohydrogels based on chitosan and silicon glycerolates were synthesized by a sol–gel method; the effect of silicon glycerolates and chitosan concentrations on the process of gel formation was evaluated.

\\\\expert2\\nbo\\Mendeleev Communications\\2014, v.24, p. 201-202.pdf
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   I-70


    Investigation of Regularities, Mechanism of Formation, and Structure of Hydrogels based on Silicon and Titanium Polyolates / T. G. Khonina, M. V. Ivanenko, E. V. Shadrina, O. N. Chupakhin // Третья международная конференция стран СНГ «Золь-гель 2014», Суздаль, 8–12 сентября 2014 г. : тез. докл. - Суздаль, 2014. - С. 24

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
HYDROGELS -- TITANIUM POLYOLATES -- SILICON POLYOLATES

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   M 61


    Metal and silicon oxides as efficient catalysts for the preparative organic chemistry [Electronic resource] / Yu. A. Titova, O. V. Fedorova, G. L. Rusinov, V. N. Charushin // Russian Chemical Reviews. - 2015. - Т. 84, № 12. - С. 1294-1315. - Bibliogr. : p. 1312-1315 (189 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SILICON OXIDES -- METAL OXIDES
Аннотация: Data on the use of metal and silicon oxides as catalysts of reactions which are most in demand in laboratory organic syntheses are summarized. The potential of oxide catalysts for optimization of organic reactions is demonstrated, and some mechanistic aspects of oxide action are considered. Published data on the synthetic use of single, mixed, bulk and nanosized metal and silicon oxides are presented.

\\\\expert2\\nbo\\Russian Chemical Reviews\\2015, V.84, N12, p. 1294-1315.pdf
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   I-70


    Investigation of regularities, mechanism of formation, and structure of hydrogels based on silicon - and titanium polyolates / T. G. Khonina, M. V. Ivanenko, E. V. Shadrina, O. N. Chupakhin // Третья международная конф. стран СНГ "Золь-гель синтез и исследование неорганических соединений, гибридных функциональных материалов и гибридных систем" "Золь-гель 2014", Суздаль, 8-12 сентября 2014 г. : докл. - Суздаль, 2014. - С. 24. - Bibliogr. : p. 24 (2 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
HYDROGELS -- TITANIUM POLYOLATES

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   E 97


    Extraction of vanadium (IV) with DI-2-ethylhexylphosphoric acid [Электронный ресурс] / L. D. Kurbatova, P. A. Slepukhin, D. I. Kurbatov, E. V. Zabolotskaya // Phosphorus, Sulfur, and Silicon and the Related Elements. - 2012. - Vol.187, №9. - P1032-1037

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ELECTRONIC SPECTRA -- ESR SPECTROSCOPY -- VANADIUM
Аннотация: It was established with the use of electron and ESR spectroscopic methods that in the presence of sodium sulfate, the extraction of vanadium (IV) with di-2-ethylhexylphosphoric acid takes place by a cation-exchange mechanism giving rise to two complex compounds of vanadium (IV) oxocation with sulfuric and di-2-ethylhexylphosphoric acid anions. The vanadium (IV) oxocation sulfate complex extracted in the solid state was examined with X-ray structural analysis. It was shown that the vanadium (IV) oxocation sulfate complex trihydrate crystallizes in the centrosymmetrical space group to form dimers with bridging sulfate groups

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   S 98


    Synthesis of pharmacologically active hydrogels [Electronic resource] / M. V. Ivanenko, T. G. Khonina, O. N. Chupakhin, L. P. Larionov // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2012. - Vol.61, №11. - С. 2163-2171. - Bibliogr. : p. 2171 (30 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
SILICON POLYOLATES -- TITANIUM POLYOLATES -- WOUND-HEALING
Аннотация: The target synthesis of new biologically active hydrogels based on combined silicon and titanium polyolates was carried out. The optimum conditions for hydrogel formation and their composition were determined. The type of hydrogels and mechanisms of gelation depend on the nature of polyols: gels based on combined silicon and titanium polyethylene glycolates are polymeric and formed via the polycondensation mechanism, whereas gels based on combined silicon and titanium glycerolates are colloidal and formed via the coagulation—condensation mechanism. The combined hydrogels based on silicon dimethyl glycerolates and titanium tetraglycerolate exhibit enhanced transcutaneous, wound healing, and regenerating activity

\\\\expert2\\NBO\\Russian Chemical Bulletin\\2012, 61 (11), 2163-2171.pdf
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   N 52


    New hybrid chitosan-silicone-containing glycerohydrogels [Electronic resource] / E. Yu. Larchenko, E. V. Shadrina, T. G. Khonina, O. N. Chupakhin // Mendeleev Communications. - 2014. - Vol.24, №4. - С. 201-202. - Bibliogr. : p. 202 (20 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CHITOSAN -- GLYCEROHYDROGELS -- SOL-GEL METHOD
Аннотация: New biologically active hybrid chitosan-silicone-containing glycerohydrogels based on chitosan and silicon glycerolates were synthesized by a sol-gel method; the effect of silicon glycerolates and chitosan concentrations on the process of gel formation was evaluated.

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   S 98


    Synthesis and antimicrobial activity of silicon-titanium-zinc- and silicon-titanium-boron-containing glycerohydrogels / T. G. Khonina, E. Yu. Nikitina, E. V. Shadrina [et al.] // Russian chemical bulletin. - 2021. - Vol. 70, № 5. - P967-974

ББК Г
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Novel pharmacologically active silicon—titanium—zinc- and silicon—titanium—boron-containing glycerohydrogels were synthesized by the sol—gel method using silicon, titanium, zinc, and boron glycerolates as biocompatible precursors. The compositions and structural features of the hydrogels were studied by transmission electron microscopy, scanning electron microscopy, IR spectroscopy, atomic emission spectrometry, and elemental analysis methods. The disperse phase and liquid water—glycerol medium of the hydrogels were isolated by cold exhaustive extraction with ethanol and characterized. The 3D polymeric network of the gels is formed by the products of hydrolysis and subsequent (co)condensation of silicon-/silicon—boron-containing precursors. Titanium and zinc glycerolates undergo no hydrolytic transformations under gelation conditions and exist in the cells of the 3D polymeric network in the form of amorphous nanoparticles that are not linked to the network by covalent bonds. Models of the structures were proposed. The gels are characterized by antimicrobial activity, which is more pronounced for the silicon—titanium—boron-containing gel, and they can be considered as promising drugs for topical treatment prepared by the simple, environmentally friendly, and cost-effective method.

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    Bioactive silicon-iron-containing glycerohydrogel synthesized by the sol-gel method in the presence of chitosan / T. G. Khonina, D. S. Tishin, L. P. Larionov [et al.] // Russian chemical bulletin. - 2022. - Vol. 71, № 11. - P2342-2351
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: A novel biologically active nanocomposite glycerohydrogel based on two biocompatible precursors, silicon and iron glycerolates, was synthesized by the sol—gel method in the presence of chitosan (Ch). The composition and structural features of the gel were characterized by advanced analytical methods including transmission electron microscopy, X-ray diffraction, and atomic emission spectroscopy. It was shown that iron(iii) monoglycerolate undergoes partial hydrolysis under the gelation conditions and exists as a separate nanoscale phase along with the hydrolysis products in cells of the 3D Si-containing polymeric gel network. This network is formed as a result of incomplete hydrolysis of silicon glycerolates in excess glycerol followed by homo- and heterofunctional condensation of silanol groups with the formation of Si-O-Si units containing residual glyceroxy groups at the silicon atom. Chitosan forms numerous intermolecular bonds with the 3D gel network, accelerates the process of gelation, makes the gel morphostructure more ordered, and increases the stability of the gel. The Si-Fe-Ch-containing glycerohydrogel is nontoxic and possesses hemostatic and wound-healing activity, being a promising topical medication for medical and veterinary practice.

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10.

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    Biocompatible silica-polyethylene glycol-based composites for immobilization of microbial cells by sol-gel synthesis / D. G. Lavrova, A. N. Zvonarev, V. A. Alferov [et al.] // Polymers. - 2023. - Т. 15, № 2. - P458
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ORMOSIL COMPOSITES -- BIOFILTER -- BIOCATALYSTS
Аннотация: Biocatalysts based on the methylotrophic yeast Ogataea polymorpha VKM Y-2559 immobilized in polymer-based nanocomposites for the treatment of methanol-containing wastewater were developed. The organosilica composites with different matrix-to-filler ratios derived from TEOS/MTES in the presence of PEG (SPEG-composite) and from silicon-polyethylene glycol (STPEG-composite) differ in the structure of the silicate phase and its distribution in the composite matrix. Methods of fluorescent and scanning microscopy first confirmed the formation of an organosilica shell around living yeast cells during sol-gel bio-STPEG-composite synthesis. Biosensors based on the yeast cells immobilized in STPEG- and SPEG-composites are characterized by effective operation: the coefficient of sensitivity is 0.85 ± 0.07 mgO2 × min−1 × mmol−1 and 0.87 ± 0.05 mgO2 × min−1 × mmol−1, and the long-term stability is 10 and 15 days, respectively. The encapsulated microbial cells are protected from UV radiation and the toxic action of heavy metal ions. Biofilters based on the developed biocatalysts are characterized by high effectiveness in the utilization of methanol-rich wastewater—their oxidative power reached 900 gO2/(m3 × cycle), and their purification degree was up to 60%.

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11.

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    Synthesis and physicochemical and catalytic properties of composites in the Sio2–Zro2 system / A. N. Murashkevich, O. A. Alisienok, E. S. Novik [et al.] // Inorganic materials. - 2020. - Vol. 56, № 4. - P430-436
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ACID-BASE PROPERTIES -- CATALYSIS -- COMPOSITE -- SILICA -- SPECIFIC SURFACE AREA -- ZIRCONIA
Аннотация: Using coprecipitation, a sol–sol method, and molecular layering, we have synthesized SiO2–ZrO2 composites with SiO2 : ZrO2 ratios from 1 : 1 to 9 : 1 and a large specific surface area, which increases with growth silicon-containing component concentration. Using adsorption of Hammett indicators, we have assessed the concentration of acid–base centers in the pK range 1.3–9.6, which has been shown to vary from 68 to 160 μmol/g. Elemental analysis and IR spectroscopy data have demonstrated the presence of not only water but also nitrate ions and carbon dioxide on the surface of the samples. It has been shown that the use of nanoparticulate SiO2–ZrO2 oxides as heterogeneous catalysts—promoters for (2S,4R)-4-hydroxyprolyl-(S)-1-phenylethylamine trifluoroacetate, a chiral inducer in the asymmetric Biginelli reaction, makes it possible to raise ee (enantiomeric excess) from 39 to 68% and the reaction yield from 29 to 55%.

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12.

Инвентарный номер: нет.

   F 33


    Features of silicon- and titanium-polyethylene glycol precursors in sol-gel synthesis of new hydrogels [Electronic resource] / T. G. Khonina, A. P. Safronov, M. V. Ivanenko, E. V. Shadrina, O. N. Chupakhin // Journal of Materials Chemistry B. - 2015. - Vol. 3, № 27. - С. 5490-5500. - Bibliogr. : p. 5499-5500 (38 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
MODIFIED SILANES -- MINERALIZATION -- MONOLITHS
Аннотация: The formation of organic/inorganic hydrogels based on silicon and titanium polyethylene glycolates, new biocompatible water-soluble precursors in sol-gel processing, was investigated. The influence of different factors on the gelation process, such as excess of PEG, water molar content, pH of medium, electrolyte additives, was investigated in comparison with silicon-and titanium-glycerol precursors. The specific features of gelation for each type of precursor were revealed. It has been determined that titanium polyethylene glycolates synthesized and used in the excess of PEG formed transparent polymeric hydrogels resistant to syneresis under certain conditions. The titanium polyethylene glycolates synthesized without excess of PEG formed turbid heterogeneous colloidal gels. In the case of silicon polyethylene glycolates the hydrogels obtained were polymeric. Dynamic light scattering was used to confirm the polymeric or colloidal type of gelation. The solid and liquid phases of polymeric silicon- and titanium-polyethylene glycol hydrogels were separated by exhaustive extraction. The solid phase was characterized by combined thermal analysis with simultaneous quadruple mass spectrometry, XRD, IR spectroscopy, and liquid phase-atomic emission spectroscopy. The structural features of polymeric gels were investigated by SEM and TEM methods. The cross-linking density of polymeric hydrogels was evaluated using Flory-Rehner theory based on the mechanical properties of swollen networks of flexible polymeric chains

\\\\expert2\\nbo\\Journal of Materials Chemistry B\\2015. V. 3, N 27. P. 5490-5500.pdf
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13.

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   A 89


    Asymmetric Biginelli Reaction Catalyzed by Silicon, Titanium and Aluminum Oxides [Electronic resource] / O. V. Fedorova, Yu. A. Titova, A. Yu. Vigorov, M. S. Toropova, O. A. Alisienok, A. Murashkevich, V. P. Krasnov, G. L. Rusinov, V. N. Charushin // Catalysis Letters. - 2016. - Vol.146, № 2. - С. 493-498

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
BIGINELLI REACTION -- PHENYLETHYLAMINE -- ALUMINUM OXIDES
Аннотация: The asym. Biginelli reaction was investigated in the presence of N-[(2S,4R)-4-hydroxyprolyl]-(S)-1-phenylethylamine as chiral inducer and silicon, titanium or aluminum oxides (individual and mixed, bulk and nanosized) as heterogeneous catalysts. The synthesis of Et (4R)-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate from benzaldehyde, urea and Et acetoacetate has been described. It has been shown that all studied oxides improve chemo- and stereoselectivity of the Biginelli reaction.

\\\\expert2\\nbo\\Catalysis Letters\\2016, v.146, p.493.pdf
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14.

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   N 89

    Novoselova, M. E.
    Formation regularities of silicon-polysaccaride-containing polyolate hydrogels / M. E. Novoselova, M. V. Ivanenko, E. Yu. Nikitina, T. G. Khonina // Современные синтетические методологии для создания лекарственных препаратов и функциональных материалов (MOSM2018): вторая международная научно-практическая конференция : материалы и доклады. - Екатеринбург, 2019. - С. 120

ББК Г
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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15.

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   N 52


    New hybrid chelating sorbents with grafted 3-aminopropionate groups based on mixed silicon, aluminum, titanium, or zirconium oxides [Electronic resource] / Yu. G. Yatluk, N. A. Zhuravlev, O. V. Koryakova, L. K. Neudachina, Yu. A. Skorik // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2005. - Vol. 54, № 8. - P1836-1841

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: A series of new hybrid organo-inorganic sorbents with the 3-aminopropionate chelating group was synthesized. The synthesis includes the copolycondensation (sol—gel method) of tetraethoxysilane, 3-aminopropyltriethoxysilane, and several modifiers (MeSi(OEt)3, EtSi(OEt)3, Ti(OEt)4, AlONO3, ZrOCl2) followed by carboxyethylation with acrylic acid. The obtained chelating sorbents were characterized by elemental analysis, FT-IR and 1H NMR spectroscopy, and thermogravimetry. The N-carboxylated sorbents have a higher sorption capacity with respect to metal ions (0.5–0.9 mmol g?1, pH 6.3, NH4OAc, 20 °C) than the starting sorbents with the primary amino group (0.05–0.2 mmol g?1) and manifest high selectivity for copper(II) ion extraction

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2005, 54 (8), 1836.pdf
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16.

Инвентарный номер: нет.

   S 98


    Synthesis of hydrogels based on silicon polyolates [Electronic resource] / T. G. Khonina, E. V. Shadrina, A. A. Boyko, O. N. Chupakhin, L. P. Larionov, A. A. Volkov, V. D. Burda // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2010. - Vol. 59, № 1. - P75-80

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ORGANOSILICON COMPOUNDS -- DIOLS -- GLYCEROL
Аннотация: Biologically active hydrogels based on silicon polyolates, which are the products of reactions of tetraethoxy- and methyltriethoxysilanes with polyols (1,2-propanediol, glycerol, polyethylene glycol), were synthesized. The optimal conditions for hydrogel formation and hydrogel composition were determined. The acute toxicity and transcutaneous and wound-healing activities of the synthesized compounds were studied. The experimental results show that hydrogels based on silicon polyolates can be recommended for further preclinical and clinical tests with the purpose of their use in medical practice both as self-sufficient agents and ointment bases of pharmaceutical compositions with wound-healing, regenerative, and transcutaneous action

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2010, 59 (1), 75-80.pdf
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17.

Инвентарный номер: нет.

   С 38


    Синтез, токсичность и трансдермальная проницаемость глицератов кремния и гидрогелей на их основе [] = Synthesis, toxicity, and percutaneous activity of silicon glycerolates and related hydrogels / Т. Г. Хонина, О. Н. Чупахин, Л. П. Ларионов, Т. Г. Бояковская, А. Л. Суворов, Е. В. Шадрина // Химико-фармацевтический журнал. - 2008. - № 11. - С. 5-9 : рис., табл., граф. - Библиогр.: с. 9 (12 назв.) . - ISSN 0023-1134

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
КРЕМНИЙ -- ГЛИЦЕРАТЫ КРЕМНИЯ -- ГИДРОГЕЛИ -- ГЕЛЕОБРАЗОВАНИЕ -- ПРОВОДНИКИ ТРАНСКУТАННЫЕ -- СИНТЕЗ -- ТОКСИЧНОСТЬ -- ПРОНИЦАЕМОСТЬ ТРАНСДЕРМАЛЬНАЯ

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18.

Инвентарный номер: нет.

   Э 94


    Эффективность импульсного магнитофореза в комплексной терапии хронического генерализованного пародонтита с использованием композиций на основе кремнийорганического глицерогидрогеля= Effectiveness of pulsed magnitophoresis in the complex treatment of chronic generalized periodontitis with the use of compositions based on silicon-organic glycerohydrogel [] / О. Л. Шнейдер, В. И. Баньков, Л. П. Ларионов, Т. Г. Хонина, Е. В. Шадрина, Е. А. Богданова, Н. А. Сабирзянов // Уральский медицинский журнал. - 2009. - № 5. - С. 76-80

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: В работе изложены основные результаты исследования эффективности применения нового метода лечения хронического генерализованного пародонтита посредством проведения импульсного магнитофореза разработанной лекарственной композиции на основе кремнийорганического глицерогидрогеля

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19.

Инвентарный номер: нет.

   S 90


    Study of scintillator strip with wavelength shifting fiber and silicon photomultiplier [Text] / V. Balagura, M. Danilov, B. Dolgoshein, S. Klemin, R. Mizuk, P. Pakhlov, E. Popova, V. L. Rusinov, E. Tarkovsky, I. Tikhomirov // Nuclear Instruments & Methods in Physics Research, Section A: Accelerators, Spectrometers, Detectors, and Associated Equipment. - 2006. - Vol. 564, № 1. - P590-596

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: The performance of the 200*2.5*1 cm3 plastic scintillator strip with wavelength shifting fiber read out by two novel photodetectors called Silicon PhotoMultipliers (SiPMs) is discussed. The advantages of SiPM relative to the traditional multichannel photomultiplier are shown. Light yield and light attenuation measurements are presented. This technique can be used in muon or calorimeter systems.

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20.

Инвентарный номер: нет.

   T 44

    Rusinov, V. L.
    The scintillator tile hadronic calorimeter prototype [Text] / V. L. Rusinov // Nuclear Physics B, Proceedings Supplements. - 2006. - Vol. 150: Innovative Particle and Radiation Detectors. - P253-256

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: A high granularity scintillator hadronic calorimeter prototype is described. The calorimeter is based on a novel photodetector - Silicon Photo-Multiplier (SiPM). The main parameters of SiPM are discussed as well as readout cell construction and optimization. The experience with a small prototype production and testing is described. A new 8 k channel prototype is being manufactured now.

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