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1.

Вид документа : Статья из журнала
Шифр издания : 54/S 98
Автор(ы) : Pervova I. G., Melkozerov S. A., Slepukhin P. A., Lipunova G. N., Barachevskii V. A., Lipunov I. N.
Заглавие : Synthesis, structure, and photochemical properties of hetarylaldehydes benzimidazolyl-2-hydrazones [Electronic resource]
Место публикации : Russian Journal of General Chemistry. - 2010. - Vol. 80, № 5. - С. 987-993: рис., табл.
Систем. требования: http://www.springerlink.com/content/2687338427056v14/fulltext.pdf
Примечания : 17.10.2011
ББК : 54
Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: New benzimidazolyl-2-hydrazones of 2-furaldehyde, thiophene-2-carbaldehyde and pyridine-2-carbaldehyde were synthesized and their structure was studied by H-1 NMR and X-ray analysis. Photochemical properties of these compounds and of benzothiazolyl-2-hydrazones of 2-furaldehyde, thiophene-2-carbaldehyde and pyridine-2-carbaldehyde in solutions were investigated. The process of phototransformation is determined by the nature of the aldehyde fragment of hydrazones
\\\\Expert2\\nbo\\Russian Journal of General Chemistry\\2010, V. 80, N 5, p.987.pdf
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2.

Вид документа : Статья из журнала
Шифр издания : 54/S 98
Автор(ы) : Irgashev R. A., Teslenko A. Yu., Zhilina E. F., Schepochkin A. V., Eltsov O. S., Rusinov G. L., Charushin V. N.
Заглавие : Synthesis, photophysical and electrochemical properties of novel 6,12-di(thiophen-2-yl) substituted indolo[3,2-b]carbazoles [Электронный ресурс]
Место публикации : Tetrahedron. - 2014. - Vol.70, №31. - С. 4685-4696
Систем. требования: http://www.sciencedirect.com/science/article/pii/S0040402014006395
Примечания : 08.08.2014
ББК : 54
Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ
Ключевые слова (''Своб.индексиров.''): indolo[3,2-b]carbazole--indole--thiophene
Аннотация: Novel 5,11-dialkyl-6,12-di(thiophen-2-yl) substituted 5,11-dihydroindolo[3,2-b]carbazoles have been obtained and plausible ways for their further modifications via the Friedel–Crafts reaction are presented. The formylation of these indolo[3,2-b]carbazoles with dichloromethyl alkyl esters catalysed by Lewis acids leads to the formation of the corresponding 2,8-diformyl derivatives. Applicability of this formylation method for modification of indolo[3,2-b]carbazoles bearing electron-rich aromatic substituents at C-6 and C-12 has also been demonstrated. The Knoevenagel condensation of 2,8-dialdehydes with active methylene nitriles has been studied. The measurements of optical and redox properties for a number of new indolo[3,2-b]carbazoles have been performed
\\\\expert2\\nbo\\Tetrahedron\\2014, v. 70 , p. 4685-4696.pdf
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3.

Вид документа :
Шифр издания : 54/S 98
Автор(ы) : Kudyakova Yu.S., Burgart Ya. V., Slepukhin P. A., Saloutin V. I.
Заглавие : Synthesis of New Heteroatomic Podands from Ethyl 2-[(2-Aminophenylamino)Methylidene]-3-Oxoalkanoates and Thiophene-2,5-Dicarboxaldehyde
Место публикации : Mendeleev Communications. - 2012. - Vol.22, №5. - С. 284-286
ББК : 54
Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ
Ключевые слова (''Своб.индексиров.''): heteroatomic podands --3-oxoalkanoates --dicarboxaldehyde
Аннотация: Condensation of two moles of ethyl 2-[(2-aminophenylamino)methylidene]-3-oxo-3-(polyfluoroalkyl)propionates with 2,5-thiophene-dicarboxaldehyde results in new heteroatomic podands. X-ray data showed that in the solid state these molecules arrange in two independent chelating fragments of b-amino enone type, thiophene fragment being a spacer
\\\\Expert2\\nbo\\Mendeleev Communications\\2012, v.22, p. 284.pdf
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4.

Вид документа : Статья из журнала
Шифр издания : 54/P 58
Автор(ы) : Kozhevnikov D. N., Kozhevnikov V. N., Shafikov M. Z., Prokhorov A. M., Bruce D.W., J. A. Gareth Williams
Заглавие : Phosphorescence vs Fluorescence in Cyclometalated Platinum(II) and Iridium(III) Complexes of (Oligo)thienylpyridines
Место публикации : Inorganic Chemistry . - 2011. - Vol. 50, № 8. - С. 3804-3815
ББК : 54
Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ
Ключевые слова (''Своб.индексиров.''): oligothienylpyridines--ligands--luminescence properties
Аннотация: Two newly prepared oligothienylpyridines, 5-(2-pyridyl)-5?-dodecyl-2,2?-bithiophene, HL2, and 5-(2-pyridyl)-5??-dodecyl-2,2?:5?,2??-ter-thiophene, HL3, bind to platinum(II) and iridium(III) as NC-coordinating ligands, cyclometallating at position C4 in the thiophene ring adjacent to the pyridine, leaving a chain of either one or two pendent thiophenes. The synthesis of complexes of the form [PtLn(acac)] and [Ir(Ln)2(acac)] (n = 2 or 3) is described. The absorption and luminescence properties of these four new complexes are compared with the behavior of the known complexes [PtL1(acac)] and [Ir(L1)2(acac)] {HL1 = 2-(2-thienyl)pyridine}, and the profound differences in behavior are interpreted with the aid of time-dependent density functional theory (TD-DFT) calculations. Whereas [PtL1(acac)] displays solely intense phosphorescence from a triplet state of mixed ??*/MLCT character, the phosphorescence of [PtL2(acac)] and [PtL3(acac)] is weak, strongly red shifted, and accompanied by higher-energy fluorescence. TD-DFT reveals that this difference is probably due to the metal character in the lowest-energy excited states being strongly attenuated upon introduction of the additional thienyl rings, such that the spin?orbit coupling effect of the metal in promoting intersystem crossing is reduced. A similar pattern of behavior is observed for the iridium complexes, except that the changeover to dual emission is delayed to the terthiophene complex [Ir(L3)2(acac)], reflecting the higher degree of metal character in the frontier orbitals of the iridium complexes than their platinum counterparts.??
\\\\Expert2\\nbo\\Inorganic Chemistry\\2011, v.50, p.3804.pdf
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5.

Вид документа : Статья из журнала
Шифр издания : 54/N 89
Автор(ы) : Irgashev R. A., Karmatsky A. A., Kim G. A., Rusinov G. L., Charushin V. N., Sadovnikov A. A., Ivanov V. K., Kozyukhin S. A., Emets V. V., Grinberg V. A.
Заглавие : Novel push-pull thieno[2,3-b]indole-based dyes for efficient dye-sensitized solar cells (DSSCs)
Место публикации : Arkivoc. - 2017. - Vol. 4. - С. 34-50
ББК : 54
Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ
Ключевые слова (''Своб.индексиров.''): dye-sensitized solar cells--electron-rich heterocycles--metal-free dyes--photovoltaic properties--push-pull structure--thieno[2,3-b]indole
Аннотация: New metal-free sensitizers (IK 3-6), based on the thieno[2,3-b]indole ring system, bearing various aliphatic substituents at the nitrogen atom (electron-donating part), several thiophene units (π-bridge linker) and 2-cyanoacrylic acid (the electron-accepting and anchoring group) have been synthesized for application in dye-sensitized solar cells (DSSCs). The relationship between the IK dye structure and efficiency of the corresponding DSSC has been elucidated. Power conversion efficiency (PCE) up to 6.3% (short-circuit photocurrent density (JSC) 19.0 mA cm-2, open-circuit voltage (VOC) 0.59 V, and fill factor (FF) 56.4%) were obtained for the DSSC, based on 2-cyano-3-{5-[8-(2-ethylhexyl)-8H-thieno[2,3-b]indol-2-yl]thiophen-2-yl}acrylic acid (IK 3), which proved to be a highly synthetic available compound, under simulated AM 1.5 G irradiation (100 mW cm-2), thus indicating that thieno[2,3-b]indole-based organic dyes are perspective candidates for DSSCs.
\\\\Expert2\\NBO\\ARKIVOC\\2017 v.4 p.34-50.pdf
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6.

Вид документа : Статья из журнала
Шифр издания : 54/N 52
Автор(ы) : Verbitskiy E. V., Baranova A. A., Lugovik K. I., Khokhlov K. O., Cheprakova E. M., Shafikov M. Z., Rusinov G. L., Chupakhin O. N., Charushin V. N.
Заглавие : New 4,5-di(hetero)arylpyrimidines as sensing elements for detection of nitroaromatic explosives in vapor phase
Место публикации : Dyes and Pigments. - 2017. - Vol. 137. - С. 360-371
ББК : 54
Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ
Ключевые слова (''Своб.индексиров.''): fluorescence quenching--nitroaromatic explosives--triphenylamines--carbazoles--pyrimidines
Аннотация: A series of D–π–A–π–D type dyes based on pyrimidines, bearing thiophene linkers, have been studied as sensing fluorophores. Fluorescence studies have demonstrated that the emission of all derivatives is sensitive to the presence of 2,4,6-trinitrotoluene (TNT) and other nitroaromatic compounds (NACs), in their acetonitrile solutions. The detection limits of fluorophores to NACs proved to be in the range from 10−4 to 10−6 mol/L. The time-resolved fluorescence measurements and theoretical investigation into the quenching mechanism in the presence of fluorophore has been performed. The two types of sensor prototypes for handheld sniffer «Nitroscan» (Plant «Promautomatika», Ekaterinburg, Russia) on the basis of non-woven dry wipe and spunlace non-woven fabric with various quantities of the most sensitive fluorophore have been fabricated. The reusable, reversible and sensitive response of the designed prototypes to NACs enables one to qualify these compounds as promising fluorescent sensory materials for detection of NACs.
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7.

Вид документа : Статья из журнала
Шифр издания : 54/N 52
Автор(ы) : Verbitskiy E. V., Baranova A. A., Lugovik K. I., Khokhlov K. O., Cheprakova E. M., Shafikov M. Z., Rusinov G. L., Chupakhin O. N., Charushin V. N.
Заглавие : New 4,5-di(hetero)arylpyrimidines as sensing elements for detection of nitroaromatic explosives in vapor phase
Место публикации : Dyes and Pigments. - 2016. - Vol. 137. - С. 360-371
Примечания : Bibliogr. : p. 370-371 (50 ref.)
ББК : 54
Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ
Ключевые слова (''Своб.индексиров.''): 4,5-di(hetero)arylpyrimidines --nitroaromatic explosives --vapor phase
Аннотация: A series of D–π–A–π–D type dyes based on pyrimidines, bearing thiophene linkers, have been studied as sensing fluorophores. Fluorescence studies have demonstrated that the emission of all derivatives is sensitive to the presence of 2,4,6-trinitrotoluene (TNT) and other nitroaromatic compounds (NACs), in their acetonitrile solutions. The detection limits of fluorophores to NACs proved to be in the range from 10−4 to 10−6 mol/L. The time-resolved fluorescence measurements and theoretical investigation into the quenching mechanism in the presence of fluorophore has been performed. The two types of sensor prototypes for handheld sniffer «Nitroscan» (Plant «Promautomatika», Ekaterinburg, Russia) on the basis of non-woven dry wipe and spunlace non-woven fabric with various quantities of the most sensitive fluorophore have been fabricated. The reusable, reversible and sensitive response of the designed prototypes to NACs enables one to qualify these compounds as promising fluorescent sensory materials for detection of NACs.
\\\\expert2\\nbo\\Dyes and Pigments\\2016, v. 137, p.360-371.pdf
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8.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Filatova E. S., Fedorova O. V., Chistyakov K. A., Rusinov G. L., Charushin V. N.
Заглавие : Features of a multicomponent biginelli reaction involving 3-oxobutanoyl-containing podands, aromatic aldehydes, and 1,2,4-triazol-3-amine
Место публикации : Chemistry of heterocyclic compounds. - 2020. - Vol. 56, № 1. - С. 88-91
Ключевые слова (''Своб.индексиров.''): dihydropyrimidine--monosubstituted podand--podand--triazolo[1,5-а]pyrimidine--triazolo[4,3-а]pyrimidine--tuberculostatic activity
Аннотация: [Figure not available: see fulltext.] A reaction of 3-oxobutanoyl-containing podands with thiophene-2-carbaldehyde (or benzaldehyde) and 3-amino-1,2,4-triazole gave podands featuring a 4,7-dihydro[1,2,4]triazolo[1,5-а]pyrimidine motif. It was established that the process was accompanied by the formation of [4,3-а]-isomers, which occurred in a slight excess during the synthesis of a podand containing a phenyl group at position 7 and, on the other hand, were observed as the minor products during the synthesis of podands bearing a thiophen-2-yl substituent. Trace amounts of monosubstituted podands were also detected, containing a free hydroxy group along with the triazolodihydropyrimidine pharmacophore.
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9.

Вид документа : Статья из журнала
Шифр издания : 54/D 47
Автор(ы) : Verbitskiy E. V., Baranova A. A., Ludovik K. I., Shafikov M. Z., Khokhlov K. O., Cheprakova E. M., Rusinov G. L., Chupakhin O. N., Charushin V. N.
Заглавие : Detection of nitroaromatic explosives by new D-π-A sensing fluorophores on the basis of the pyrimidine scaffold [Электронный ресурс]
Место публикации : Analytical and Bioanalytical Chemistry. - 2016. - С. Ahead of Print
Систем. требования: springer.com/search?query=10.1007%2Fs00216-016-9501-4
Примечания : 06.04.16
ББК : 54
Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ
Ключевые слова (''Своб.индексиров.''): nitroaromatic explosives--pyrimidine scaffold
Аннотация: A series of D-​π-​A- type dyes based on pyrimidines, bearing various thiophene linkers, have been studied as sensing fluorophores. Fluorescence studies have demonstrated that the emission of all derivs. is sensitive to the presence of nitroarom. explosives, such as 2,​4,​6-​trinitrophenol (PA)​, 2,​4,​6-​trinitrotoluene (TNT)​, and 2,​4-​dinitrotoluene (DNT)​, in their acetonitrile solns. The detection limits of fluorophores to PA, TNT, and DNT proved to be in the range from 5.83 × 10-​6 to 2.38 × 10-​7 mol​/L, 1.70 × 10-​4 to 8.40 × 10-​6 mol​/L, and 8.39 × 10-​5 to 6.87 × 10-​6 mol​/L, resp. The theor. investigation into the quenching mechanism in the presence of fluorophore has been performed. All compds. have shown a good efficiency as sensor materials when tested as elements of the original device Nitroscan for detecting nitro-​contg. explosives in vapor phase
\\\\expert2\\nbo\\Analytical and Bioanalytical Chemistry\\2016, Ahead Print.pdf
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10.

Вид документа : Статья из журнала
Шифр издания : 54/C 75
Автор(ы) : Irgashev R. A., Karmatsky A. A., Rusinov G. L., Charushin V. N.
Заглавие : Construction of Heteroacenes with Fused Thiophene and Pyrrole Rings via the Fischer Indolization Reaction
Место публикации : Organic Letters. - 2016. - Vol. 18, № 4. - С. 804-807
ББК : 54
Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ
Ключевые слова (''Своб.индексиров.''): fused thiophene--pyrrole rings--fischer indolization reaction
Аннотация: A convenient approach to ladder-type 6H-benzo[4',5']thieno[2',3':4,5]thieno[3,2-b]indoles, e.g., I (X-rays single crystal structure shown)​, bearing various substituents in both terminal benzene rings has been developed. The protocol suggested for prepg. these N,S-​heteroacenes is based on using easily available reagents, such as cinnamic acids and arylhydrazines, which can be involved in the Fischer indole synthesis, as the key step. A similar condensed system of 12H-​benzo[4'',​5'']​thieno[2'',3'':4',5']​thieno[2',3':4,5]​thieno[3,2-b]indole, bearing six rings, has also been obtained.
\\\\expert2\\nbo\\Organic Letters\\2016, v.18, N 4, p.804-807,pdf.pdf
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