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1.
Инвентарный номер: нет.
   
   T 44

   
    The C-C coupling of ferrocenes with electron-deficlent azaaromatics - a new route for construction of heterocyclic ligands and complexes [] / O. N. Chupakhin, I. S. Kovalev, I. A. Utepova, V. L. Rusinov, V. N. Charushin // 20-th International Congress of Heterocyclic Chemistry, Palermo, July 31-August 5, 2005 : book of abstracts . - Palermo, Italy, 2005. - С. 507. - Библиогр.: с. 507 (3 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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2.
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   H 62

   
    Heterospin complexes based on dinuclear CuII triketonate and nitroxides [Electronic resource] / V. Ovcharenko, S. V. Fokin, G. V. Romanenko, V. Ikorskii, R. S. Sagdeev, D. S. Yachevskii, D. L. Chizhov, V. N. Charushin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2006. - Vol. 55, № 11. - P1904-1908
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Heterospin complexes of bis(?2-1,1,2,2,8,8,9,9-octafluorononane-3,5,7-trionato)dicopper(II) ([Cu2L2]) with nitronyl nitroxides 2-(1-methyl-1H-pyrazol-4-yl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazole-1-oxyl 3-oxide (2) and 4,4,5,5-tetramethyl-2-(3-pyridinyl)-4,5-dihydro-1H-imidazole-1-oxyl 3-oxide (1) were synthesized and structurally characterized. Crystals of the complexes are formed by the discrete bis[1-methyl-4-(4,4,5,5-tetramethyl-3-oxide-1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-1H-pyrazole]-bis (?2-1,1,2,2,8,8,9,9-octafluorononane-3,5,7-trionato)dicopper(II) etherate (3) and bis[3-(4,4,5,5-tetramethyl-3-oxide-1-oxyl-4,5-dihydro-1H-imidazol-2-yl)pyridine]-bis (?2-1,1,2,2,8,8,9,9-octafluorononane-3,5,7-trionato)dicopper(II) (4) molecules. Each Cu atom of the dinuclear chelate fragment coordinates one paramagnetic ligand through the N atom of the pyrazole or pyridine fragment, respectively. In complex 3, the paramagnetic ligands are located on one side of the plane of the chelate fragment, whereas the ligands in complex 4 are located above and below the plane of the chelate fragment. The magnetic properties of complexes 3 and 4 are determined by dominant antiferromagnetic exchange interactions between the unpaired electrons of the CuII atoms in the dinuclear Cu2L2 moiety

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2006, 55 (11), 1904.pdf
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3.
Инвентарный номер: нет.
   
   F 70

   
    Fluorinated lithium 1,3-diketonates as reagents to modify podands and crown-ethers [Electronic resource] / N. S. Boltacheva, O. V. Fedorova, I. G. Ovchinnikova, O. N. Kazheva, A. N. Chekhlov, O. A. Dyachenko, G. L. Rusinov, V. I. Filyakova, V. N. Charushin // Journal of Fluorine Chemistry. - 2007. - Vol. 128, № 7. - P762-768
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Fluorinated enaminoketones, a new type of ligands, bearing two independent coordination centers (polyether's and fluorinated enaminoketones fragments) have been obtained. The crystal structure of the Cu(II) complex of 1,5-bis-[2-(4`,4`,4`-trifluoro-1`-methyl-3`oxo-but-1`-enylamino)-phenoxy]-3-oxapentane (10) has been elucidated by X-ray crystallography. The results obtained show that the complex 10 consists of two crystallographically independent molecules C26H24CuF6N2O5 (A and B), and the metal atom in the complex 10 has four-coordinated arrangement, as a polyhedron with a distorted square with two nitrogen and two oxygen atoms located in corners.

\\\\expert2\\nbo\\Journal of Fluorine Chemistry\\2007, v.128. p.762.pdf
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4.
Инвентарный номер: нет.
   

   
    2,6-Bis(5-trifluoromethylpyrazol-3-yl)pyridine : complexation with selected d-metals [Text] : доклад, тезисы доклада / E. F. Khmara, D. L. Chizhov, A. A. Sidorov, G. G. Alexandrov, V. I. Filyakova, G. L. Rusinov, I. L. Eremenko, V. N. Charushin // International conference "Topical Problems of Organometallic and Coordination Chemistry", V Razuvaev lectures, N. Novgorod, September 3-9 2010 : book of abstracts . - Nizhny Novgorod, 2010. - P34 : рис. - Bibliogr. : p. 34 (2 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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5.
Инвентарный номер: нет.
   
   S 98

   
    Synthesis, structures, and magnetic properties of crystals of dinuclear copper(II) and cobalt(II) complexes with 3-(3,5-dimethylpyrazol-1-yl)-6-R-1,2,4,5-tetrazines [Electronic resource] / E. V. Cherdantseva, D. V. Starichenko, P. A. Slepukhin, R. I. Ishmetova, Yu. N. Shvachko, A. V. Korolev, G. L. Rusinov, V. V. Ustinov, A. I. Matern, V. N. Charushin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2010. - Vol. 59, № 4. - P717-723
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
DINUCLEAR COMPLEXES -- SPIN MAGNETISM -- TETRAZINES
Аннотация: Dinuclear complexes of CuII with 3-(3,5-dimethylpyrazol-1-yl)-6-(2-hydroxyethylami-no)-1,2,4,5-tetrazine (1) and CoII with 3-(3,5-dimethylpyrazol-1-yl)-6-(piperidin-1-yl)-1,2,4,5- tetrazine (2) were synthesized and structurally characterized, and the magnetic (SQUID) and resonance (EPR) properties of van der Waals crystals based on these complexes were studied. Unusual behavior of the effective magnetic moment ?eff(T) is observed at T < 60 K. A nonmonotonic increase in eff() for 1 (s~6 %) and a 20% reduction of eff for 2 have a common origin and are due to the influence of spin-orbital coupling on the character of the splitting between the t2g and eg levels of the central ion. Distortions of the coordination site “switch on” a positive (1) or negative (2) contribution of the orbital magnetic moment near 6 K. Irreversible temperature behavior of eff(T) in the heating and cooling regimes in the vicinity of 60 K suggests that the character of structural distortions and the magnetic properties are related to ligand geometry. This factor plays a significant role in crystal engineering of magnetoactive structures with polynitrogen ligands

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2010, 59 (4), 717-723.pdf
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6.
Инвентарный номер: нет.
   
   C 51

   
    Chelates of fluoroalkyl containing enaminoketones [Electronic resource] / V. I. Filyakova, D. L. Chizhov, E. F. Khmara, V. N. Charushin // Russian Journal of General Chemistry. - 2010. - Vol. 80, № 1. - P190-201
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: The structure and areas of practical application of fluoroalkyl containing enaminoketone chelates with d-metals are reviewed. Synthesis of ligands and the routes to the regioisomeric enaminoketones are also considered

\\\\Expert2\\nbo\\Russian Journal of General Chemistry\\2010, V. 80, N 1, p.190.pdf
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7.
Инвентарный номер: нет.
   
   N 50

   
    Neutral tetranuclear Cu(II) complex of 2,6-di(5-trifluoromethylpyrazol-3-yl)pyridine: Synthesis, characterization and its transformation with selected aza-ligands [Электронный ресурс] / E. F. Zhilina, D. L. Chizhov, A. A. Sidorov, G. G. Aleksandrov, M. Kiskin, P. A. Slepukhin, M. Fedin, V. N. Charushin // Polyhedron. - 2013. - Vol.53. - P122-131
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
COPPER (II) COMPLEX -- X-RAY -- MAGNETIC PROPERTIES
Аннотация: New tetranuclear Cu(II) complex [Cu4(L)4]·MeCN (1) with 2,6-di(5-trifluoromethyl-1H-pyrazol-3-yl)pyridine (H2L) was synthesized. It has been shown that treatment of 1 with selected aza-ligands (pyridine, 2,2′- and 4,4′-bipyridyl, 2,3,5,6-tetra-(pyridine-2-yl)pyrazine, 2,2′;6′,2″-terpyridine and 1,4-diazabicyclo[2.2.2]octane) leads to formation of other Cu(II) complexes with different nuclearity: [Cu(L)py2] (2), [Cu(L)(2,2′-bpy)] (3), [Cu(L)2(tppz)]·THF (5), [Cu(L)tpy]·C6H5CN (4), {[Cu2(L)2(4,4′-bpy)2]·(C6H5CH3)·MeCN}n (6) and {[Cu(L)DABCO]·2MeCN}n (7). Obtained compounds were characterized by IR spectroscopy, X-ray crystallography data, EPR and SQUID magnetic measurements. --------------------------------------------------------------------------------

\\\\Expert2\\NBO\\Polyhedron\\2013. v.53. p.122.pdf
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8.
Инвентарный номер: нет.
   
   T 98

   
    Two Approaches in the Synthesis of Planar Chiral Azinylferrocenes [Electronic resource] / I. A. Utepova, O. N. Chupakhin, P. O. Serebrennikova, A. A Musikhina, V. N. Charushin // Journal of Organic Chemistry. - 2014. - Vol. 79, № 18. - С. 8659-8667. - Bibliogr. : p. 8666-8667 (34 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CHIRAL AZINYLFERROCENES -- CROSS-COUPLING REACTION -- HALOGENATED AZINES
Аннотация: Two synthetic routes to the chiral azinylferrocenes (CAFs) 5 and 15, key intermediates for the synthesis of new enantiomerically enriched P,N-ligands, have been compared. The first approach is based on the palladium-catalyzed cross-coupling reaction of halogenated azines with organozinc derivatives of ferrocenes (the Negishi reaction). The second approach exploits a new synthetic methodology, which provides a shorter pathway, through the direct C–H functionalization of aromatics by the C–C coupling of halogen-free (hetero)arenes with lithium ferrocenes bearing stereogenic C and S atoms. The palladium complexes of P,N-ligands have been used as catalysts for the Tsuji–Trost reaction, which proceeds with high enantioselectivity to give allylic substitution products in good yields.

\\\\expert2\\nbo\\Journal of Organic Chemistry\\2014, v.79, p.8659.pdf
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9.
Инвентарный номер: нет.
   
   N 58

   
    Nickel(II) and copper(II) complexes based on N-(2-Carboxyethyl) alkanolamines: Influence of the amino alcohol structure on the coordination sphere of the metal center [Electronic resource] / A. V. Pestov, P. A. Slepukhin, O. V. Koryakova, V. N. Charushin // Russian Journal of Coordination Chemistry. - 2014. - Vol.40, №4. - С. 216-223. - Bibliogr. : p. 223 (28 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
NICKEL(II) COMPLEXES -- ALCOHOL STRUCTURE -- ALKANOLAMINES
Аннотация: New nickel(II) complexes based on N-(3-hydroxypropyl)-β-alanine, N-(bis(hydroxyme -thyl)methyl)-β-alanine, and N-(tris(hydroxymethyl)methyl) -β-alanine are synthesized, and their structures are studied by X-ray diffraction analysis. The coordination spheres of the nickel and copper metal centers in the condensed phase are compared for a series of N-substituted β-alaninate ligands with the regularly changed dentate mode. In the case of the copper(II) complexes, an increase in the size of the alkanolamine chelate ring or the number of hydroxymethyl groups provides the formation of achiral coordination struc -tures, whereas the structures of the nickel(II) complexes are independent of the size of the lkanolamine che -late ring or the number of hydroxymethyl groups, thus providing the formation of the complexes as racemic modifications

\\\\expert2\\nbo\\Russian Journal of Coordination Chemistry\\2014, v. 40, N. 4, p.216.pdf
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10.
Инвентарный номер: нет.
   
   P 49

    Pestov, A. V.
    Copper and nickel chelate complexes with polydentate N,O-ligands: structure and magnetic properties of polynuclear complexes [Electronic resource] / A. V. Pestov, P. A. Slepukhin, V. N. Charushin // Russian Chemical Reviews. - 2015. - Vol. 84, № 3. - С. 310-333. - Bibliogr. : p. 331-333(182 ref.)
ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
HYDROGEN-BONDED BRIDGES -- RAY CRYSTAL-STRUCTURE -- SCHIFF-BASE LIGAND
Аннотация: A comparative analysis of the structures of copper(II) and nickel(II) chelate complexes with N-substituted 2-aminoethanols, 3-aminopropan- 1 -ols, glycines and beta-alanines is performed. It is shown that tetradentate ligands based on 3-aminopropan- 1 -ol and P-alanine, sterically hindered 2-aminoethanol derivatives and tridentate enamino ketone derivatives tend to form oligonuclear copper(II) and nickel(II) complexes. Glycine derivatives do not provide the formation of oligonuclear copper(II) and nickel(II) complexes. The magnetic properties of a number of polynuclear complexes are compared.

\\\\expert2\\nbo\\Russian Chemical Reviews\\2015, V.84, N38, p. 310-333.pdf
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